N-羧氧苄基-L-谷氨酸甲酯合成路线 (共 38 条)
反应条件
sodium methylate in methanol Heating;
参考文献
Bailey, Patrick D.; Bryans, Justin S.
Tetrahedron Letters, 1988 , vol. 29, # 18 p. 2231 - 2234
反应条件
triethylamine; 4-(N,N-dimethlyamino)pyridine in dichloromethane T=0°C; 2 h; without cat., 2h; Yields of byproduct given;
参考文献
Jouin, P.; Castro, B.; Zeggaf, C.; Pantaloni, A.; Senet, J.P; et al
Tetrahedron Letters, 1987 , vol. 28, # 15 p. 1665 - 1668
反应条件
triethylamine; 4-(N,N-dimethlyamino)pyridine in dichloromethane T=0°C; 1 h; without cat., 2h; Yields of byproduct given;
参考文献
Jouin, P.; Castro, B.; Zeggaf, C.; Pantaloni, A.; Senet, J.P; et al
Tetrahedron Letters, 1987 , vol. 28, # 15 p. 1665 - 1668
反应条件
1: With tert.-butylnitrite in acetonitrile 1.5 h; Reflux; 2: With water
参考文献
Ottersbach, Philipp A.; Schmitz, Janina; Schnakenburg, Gregor; Guetschow, Michael
Organic Letters, 2013 , vol. 15, # 3 p. 448 - 451
反应条件
tert.-butylnitrite in acetonitrile 1.5 h; Heating;
参考文献
Chemical Communications, , # 3 p. 349 - 350
反应条件
triethylamine; 4-(N,N-dimethlyamino)pyridine in dichloromethane T=0°C; 1 h; without DMAP; Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 28, # 15 p. 1665 - 1668
反应条件
1: p-TSA 2: NaOMe / methanol View Scheme
参考文献
Tetrahedron Letters, , vol. 42, # 37 p. 6603 - 6606
反应条件
trifluoroacetic acid in dichloromethane T=20°C; 1 h; Title compound not separated from byproducts;
参考文献
Organic and Biomolecular Chemistry, , vol. 4, # 2 p. 211 - 223
反应条件
tert.-butylnitrite 1.5 h; Heating;
参考文献
Chemical Communications, , # 3 p. 349 - 350
反应条件
1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 24 h / 20 °C 2: tert.-butylnitrite / acetonitrile / 1.5 h / |Reflux View Scheme
参考文献
Organic Letters, , vol. 15, # 3 p. 448 - 451