1: 2,2-diphenyl-[1,3]-dithiolane With n-butyllithium in tetrahydrofuran
T=-78°C; 1 h;
2: monobromonitromethane in tetrahydrofuran
T=20°C; 10 h;
3: With aluminum oxide in tetrahydrofuran
T=20°C; 0.5 h;
phosphonic acid diethyl ester
T=150°C; Yields of byproduct given;
参考文献
Russell, Glen A.; Yao, Ching-Fa; Tashtoush, Hasan I.; Russell, June E.; Dedolph, Douglas F.
Journal of Organic Chemistry, 1991 , vol. 56, # 2 p. 663 - 669
