2-羟基-2,6-二乙基-N-甲氧基甲基乙酰苯胺合成路线 （共 5 条）
反应条件
sodium hydroxide in tetrahydrofuran
T=20°C; Hydrolysis; 0.25 h;
参考文献
Chiron, Serge; Abian, Joaquin; Ferrer, Marta; Sanchez-Baeza, Francisco
Environmental Toxicology and Chemistry, 1995 , vol. 14, # 8 p. 1287 - 1298
反应条件
1.1: 80 percent / CH2Cl2 / 36 h / -20 °C
2.1: NaH / tetrahydrofuran / 0.5 h / -20 °C
2.2: 68 percent / tetrahydrofuran / 2 h / 20 °C
3.1: 89 percent / aq. NaOH / tetrahydrofuran / 0.25 h / 20 °C
View Scheme
参考文献
Chiron, Serge; Abian, Joaquin; Ferrer, Marta; Sanchez-Baeza, Francisco
Environmental Toxicology and Chemistry, 1995 , vol. 14, # 8 p. 1287 - 1298
反应条件
1.1: NaH / tetrahydrofuran / 0.5 h / -20 °C
1.2: 68 percent / tetrahydrofuran / 2 h / 20 °C
2.1: 89 percent / aq. NaOH / tetrahydrofuran / 0.25 h / 20 °C
View Scheme
参考文献
Chiron, Serge; Abian, Joaquin; Ferrer, Marta; Sanchez-Baeza, Francisco
Environmental Toxicology and Chemistry, 1995 , vol. 14, # 8 p. 1287 - 1298
反应条件
sodium hydroxide in acetone
Substitution; 8 h; Heating;
参考文献
Potter; Carpenter
Environmental Science and Technology, 1995 , vol. 29, # 6 p. 1557 - 1563
反应条件
in acetonitrile; benzene
Irradiationvar. solvent mixtures; Rate constantMechanism;
参考文献
Schmidt, Walter F.; Hapeman, Cathleen J.; Waters, Rolland M.; Johnson, W. E.
Journal of Agricultural and Food Chemistry, 1995 , vol. 43, # 6 p. 1724 - 1729
