3-溴环己-2-烯-1-酮合成路线 （共 34 条）
反应条件
triethylamine; dibromotriphenyl-phosphorane in benzene 3 h; Ambient temperature;
参考文献
Piers, Edward; Grierson, John R.; Lau, Cheuk Kun; Nagakura, Isao
Canadian Journal of Chemistry, 1982 , vol. 60, p. 210 - 223
反应条件
BzNEt3Br; boron trifluoride diethyl etherate in dichloromethane 0.75 h; Ambient temperature;
参考文献
Kowalski, Conrad J.; Fields, Kevin W.
Journal of Organic Chemistry, 1981 , vol. 46, p. 197 - 201
反应条件
CrO3-3.5-dimethylpyrazole
参考文献
Frost, Christopher; Linnane, Patrick; Magnus, Philip; Spyvee, Mark
Tetrahedron Letters, 1996 , vol. 37, # 51 p. 9139 - 9142
反应条件
formaldehyd; hydrogen bromide in diethyl ether 1 h;
参考文献
Fischer, Hans; Klippe, Michael; Lerche, Holger; Severin, Theodor; Wanninger, Gabriele
Chemische Berichte, 1990 , vol. 123, # 2 p. 399 - 404
反应条件
formaldehyd; hydrogen bromide in diethyl ether 1 h;
参考文献
Fischer, Hans; Klippe, Michael; Lerche, Holger; Severin, Theodor; Wanninger, Gabriele
Chemische Berichte, 1990 , vol. 123, # 2 p. 399 - 404
反应条件
formaldehyd; hydrogen bromide in tetrahydrofuran 1 h;
参考文献
Fischer, Hans; Klippe, Michael; Lerche, Holger; Severin, Theodor; Wanninger, Gabriele
Chemische Berichte, 1990 , vol. 123, # 2 p. 399 - 404
反应条件
1: 81 percent / CH3COONa / ethanol / 1 h / Heating 2: 86 percent / Br2 / CH2Cl2; H2O / 12 h / Ambient temperature 3: 73 percent Chromat. / 48percent aq. HBr, 38percent aq. Formaldehyd / tetrahydrofuran / 1 h View Scheme
参考文献
Chemische Berichte, , vol. 123, # 2 p. 399 - 404
反应条件
1: Br2 / CH2Cl2 / 0.17 h / -10 °C 2: triethylamine / CH2Cl2 / 12 h / Ambient temperature 3: 80 percent Chromat. / 48percent aq. HBr, 10percent aq. Formaldehyd / diethyl ether / 1 h View Scheme
参考文献
Chemische Berichte, , vol. 123, # 2 p. 399 - 404
反应条件
1: bromine / CH2Cl2 / 0.17 h / -10 °C 2: triethylamine / CH2Cl2 / 1 h / Ambient temperature 3: 69 percent Chromat. / 48percent aq. HBr, 10percent aq. Formaldehyd / diethyl ether / 1 h View Scheme
参考文献
Chemische Berichte, , vol. 123, # 2 p. 399 - 404
反应条件
1: triethylamine / CH2Cl2 / 1 h / Ambient temperature 2: 69 percent Chromat. / 48percent aq. HBr, 10percent aq. Formaldehyd / diethyl ether / 1 h View Scheme
参考文献
Chemische Berichte, , vol. 123, # 2 p. 399 - 404
