3-氨基甲基-6-甲基吡啶合成路线 (共 5 条)
反应条件
hydrogen; nickel in acetic acid P=258.6 Torr; 4 h;
参考文献
Liu, Mao-Chin; Lin, Tai-Shun; Cory, Joseph G.; Cory, Ann H.; Sartorelli, Alan C.
Journal of Medicinal Chemistry, 1996 , vol. 39, # 13 p. 2586 - 2593
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=60°C; 24.75 h;
参考文献
JERINI AG
Patent: WO2006/128670 A1, 2006 ;
Location in patent: Page/Page column 113 ;
WO 2006/128670 A1
反应条件
hydrogenchloride; palladium on activated charcoal Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 69, p. 2574,2577
反应条件
1: PCl5 2: palladium/charcoal; ethanolic HCl / Hydrogenation View Scheme
参考文献
Journal of the American Chemical Society, , vol. 69, p. 2574,2577
反应条件
sulfuric acid; sodium nitrite
参考文献
Graf
Journal fuer Praktische Chemie (Leipzig), 1936 , vol. <2> 146, p. 88,102
Full Text Show Details
Perez-Medina et al.
Journal of the American Chemical Society, 1947 , vol. 69, p. 2574,2577