5-Alpha-胆甾烷-3-酮合成路线 (共 116 条)
反应条件
silica gel; tin(ll) chloride in tetrahydrofuran 0.133333 h; microwave irradiation;
参考文献
Das, Nalin B.; Nayak, Amalendu; Nanda, Bhagabat
Journal of Chemical Research, 2004 , # 10 p. 712 - 713
反应条件
3,3-dimethyldioxirane in acetone 18 h; Ambient temperature;
参考文献
Van Heerden; Dixon; Holzapfel
Tetrahedron Letters, 1992 , vol. 33, # 48 p. 7399 - 7402
反应条件
N-bromosuccinmide in various solvent(s) Ambient temperaturemercuric acetate was also used;
参考文献
Wu, Zufan; Mootoo, D. R.; Fraser-Reid, Bert
Tetrahedron Letters, 1988 , vol. 29, # 50 p. 6549 - 6552
反应条件
benzeneseleninic anhydride in tetrahydrofuran T=40°C; 18.5 h;
参考文献
Cussans, Nigel J.; Ley, Steven V.; Barton, Derek H. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1654 - 1657
反应条件
copper(II) sulfate in tetrahydrofuran; methanol; water 47 h; Heating;
参考文献
Attanasi, Orazio; Gasperoni, Simonetta; Carletti, Claudio
Journal fuer Praktische Chemie (Leipzig), 1980 , vol. 322, # 6 p. 1063 - 1066
反应条件
3 A molecular sieve; thiamine diphosphate; diethylazodicarboxylate in benzene T=80°C; 15 h;
参考文献
Penz, Gottfried; Zbiral, Erich
Monatshefte fuer Chemie, 1981 , vol. 112, p. 1045 - 1054
反应条件
copper(II) sulfate in tetrahydrofuran; methanol; water 22 h; Heating;
参考文献
Attanasi, Orazio; Gasperoni, Simonetta; Carletti, Claudio
Journal fuer Praktische Chemie (Leipzig), 1980 , vol. 322, # 6 p. 1063 - 1066
反应条件
benzeneseleninic anhydride in tetrahydrofuran 16 h; Ambient temperature;
参考文献
Cussans, Nigel J.; Ley, Steven V.; Barton, Derek H. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1654 - 1657
反应条件
in hexane T=20°C; Dehydroiodination; 0.3 h; Irradiation;
参考文献
Tetrahedron Letters, , vol. 40, # 52 p. 9263 - 9266
反应条件
nickel in xylene T=135 - 140°C; 4 h; Heating;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 26, p. 998 - 999