2,2',4,6,6'-五氯联苯合成路线 （共 6 条）
反应条件
1: 59 percent / Cu / 288 h / 230 °C 2: SO2Cl2, AlCl3 / CH2Cl2 / 1 h / Ambient temperature View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 29, # 6 p. 679 - 685
反应条件
1: 1.) NaNO2, aq. H2SO4, 2.) KI / 1.) 0-5 deg C, 10 min, 2.) 0 deg C, 15 min; r.t., 1 h 2: 59 percent / Cu / 288 h / 230 °C 3: SO2Cl2, AlCl3 / CH2Cl2 / 1 h / Ambient temperature View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 29, # 6 p. 679 - 685
反应条件
aluminium trichloride; sulfuryl dichloride in dichloromethane 1 h; Ambient temperature; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Organic Preparations and Procedures International, , vol. 29, # 6 p. 679 - 685
反应条件
isopentyl nitrite Cadogan modification of Gomberg-Bachman;
参考文献
Chemosphere, , vol. 31, # 2 p. 2687 - 2705
反应条件
oxygen
T=550 - 600°C; 0.00138889 h; Product distribution;
参考文献
Mazer, Thomas; Hileman, Fred D.; Noble, Roy W.; Brooks, Joseph J.
Analytical Chemistry, 1983 , vol. 55, # 1 p. 104 - 110
反应条件
oxygen
T=550 - 600°C; 0.00138889 h; Product distribution;
参考文献
Mazer, Thomas; Hileman, Fred D.; Noble, Roy W.; Brooks, Joseph J.
Analytical Chemistry, 1983 , vol. 55, # 1 p. 104 - 110
