1-苯基四氢-2(1h)-嘧啶酮合成路线 (共 5 条)
反应条件
sodium tetrahydroborate in acetic acid
1 h; Ambient temperature;
参考文献
Kashima, Choji; Katoh, Akira; Yokota, Yuko; Omote, Yoshimori
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1622 - 1625
反应条件
1,1'-carbonyldiimidazole in tetrahydrofuran; ethyl acetate
参考文献
Adir et Compagnie
Patent: US5780474 A1, 1998 ;
反应条件
ethylmagnesium bromide in tetrahydrofuran; dichloromethane
5 deg C, then 24h reflux;
参考文献
Basha, Anwer
Tetrahedron Letters, 1988 , vol. 29, # 21 p. 2525 - 2526
反应条件
1: 92 percent / CH2Cl2 / 48 h / 20 °C
2: 76 percent / tBuOK / 2-methyl-propan-2-ol / 22 h / 30 °C
View Scheme
参考文献
Meigh; Alvarez; Joule
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 17 p. 2012 - 2021
参考文献
Delaby et al.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1954 , vol. 239, p. 674