1-(3,4-二甲氧基苯基)乙醇合成路线 （共 29 条）
反应条件
(1R,2S,9S)-11-methyl-13-oxa-7,11-diazatricyclo[7.3.1.02,7]tridecane; C11H20Br2N2OPd; oxygen; caesium carbonate in chloroform T=20°C; 21.6 h; Molecular sieve; optical yield given as percent ee;
参考文献
Breuning, Matthias; Steiner, Melanie; Mehler, Christian; Paasche, Alexander; Hein, David
Journal of Organic Chemistry, 2009 , vol. 74, # 3 p. 1407 - 1410
反应条件
Nocardia corallina B-276 in octane; N,N-dimethyl-formamide T=28 - 30°C; 25 h; Enzymatic reaction;
参考文献
Perez, Herminia I.; Luna, Hector; Manjarrez, Norberto; Solis, Aida
Tetrahedron Asymmetry, 2001 , vol. 12, # 12 p. 1709 - 1712
反应条件
chlorine dioxide; sodium sulfate in water T=20 - 40°C; E(excit.); var. of pH, ionic strength; reaction in presence of chloride; Thermodynamic dataMechanismKinetics;
参考文献
Gunnarsson, N. Per-Ivar; Ljunggren, Sten C. Hj.
Acta Chemica Scandinavica, 1996 , vol. 50, # 5 p. 422 - 431
反应条件
chlorine dioxide in water T=25°C; pH=4;
参考文献
Canadian Journal of Chemistry, , vol. 80, # 7 p. 761 - 766
反应条件
1: [bis(acetoxy)iodo]benzene; Fe(TAML)Li; diphenylether / acetone / 4 h / 25 °C / |Inert atmosphere; |Green chemistry 2: bromine / chloroform / 4 h / 0 °C / |Reflux View Scheme
参考文献
Napoly, Francois; Jean-Gerard, Ludivine; Goux-Henry, Catherine; Draye, Micheline; Andrioletti, Bruno
European Journal of Organic Chemistry, 2014 , vol. 2014, # 4 p. 781 - 787
反应条件
chlorine dioxide; sodium sulfate in water
T=20 - 40°C; E(excit.); var. of pH, ionic strength; reaction in presence of chloride; Thermodynamic dataMechanismKinetics;
参考文献
Gunnarsson, N. Per-Ivar; Ljunggren, Sten C. Hj.
Acta Chemica Scandinavica, 1996 , vol. 50, # 5 p. 422 - 431
反应条件
sulfuric acid
4 h; Heating;
参考文献
Svenson, Doug; Kadla, John F.; Chang, Hou-Min; Jameel, Hasan
Canadian Journal of Chemistry, 2002 , vol. 80, # 7 p. 761 - 766
反应条件
trichlorophosphate
Condensation; 3 h; Heating;
参考文献
Koul, Surrinder; Koul, Jawahir L.; Taneja, Subhash C.; Dhar, Kanaya L.; Jamwal, Deshvir S.; Singh, Kuldeep; Reen, Rashmeet K.; Singh, Jaswant
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 1 p. 251 - 268
反应条件
1: [bis(acetoxy)iodo]benzene; Fe(TAML)Li; diphenylether / acetone / 4 h / 25 °C / |Inert atmosphere; |Green chemistry
2: bromine / chloroform / 4 h / 0 °C / |Reflux
3: sodium carbonate / N,N-dimethyl-formamide / 3 h / 25 °C
4: sodium tetrahydroborate / tetrahydrofuran; water / 0.33 h / |Reflux
5: [bis(acetoxy)iodo]benzene; Fe(TAML)Li; diphenylether; water / acetone / 1 h / 25 °C / |Green chemistry
6: 25 °C
View Scheme
参考文献
Napoly, Francois; Jean-Gerard, Ludivine; Goux-Henry, Catherine; Draye, Micheline; Andrioletti, Bruno
European Journal of Organic Chemistry, 2014 , vol. 2014, # 4 p. 781 - 787
