4-二甲胺基苯基偶氮苯磺酰氯合成路线 （共 9 条）
反应条件
phosphorus pentachloride 0.133333 h;
参考文献
Dem'yanov, P. I.; Khimenes, M. P.; Petrosyan, V. S.
Russian Journal of Physical Chemistry, 1991 , vol. 65, # 10 p. 1489 - 1493
Zhurnal Fizicheskoi Khimii, 1991 , vol. 65, p. 2808 - 2816
反应条件
ammonium hydroxide in dichloromethane T=20°C; 2 h;
参考文献
Garcia, Lidia; Pla-Quintana, Anna; Roglans, Anna
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 23 p. 5020 - 5027
反应条件
1: trichoderin A With hydrogenchloride in water T=110°C; 20 h; 2: dabsyl chloride With sodium hydrogencarbonate in acetonitrile pH=8.1;
参考文献
Pruksakorn, Patamaporn; Arai, Masayoshi; Kotoku, Naoyuki; Vilchze, Catherine; Baughn, Anthony D.; Moodley, Prashini; Jacobs Jr., William R.; Kobayashi, Motomasa
Bioorganic and Medicinal Chemistry Letters, 2010 , vol. 20, # 12 p. 3658 - 3663
反应条件
1: trichoderin A1 With hydrogenchloride in water T=110°C; 20 h; 2: dabsyl chloride With sodium hydrogencarbonate in acetonitrile pH=8.1;
参考文献
Pruksakorn, Patamaporn; Arai, Masayoshi; Kotoku, Naoyuki; Vilchze, Catherine; Baughn, Anthony D.; Moodley, Prashini; Jacobs Jr., William R.; Kobayashi, Motomasa
Bioorganic and Medicinal Chemistry Letters, 2010 , vol. 20, # 12 p. 3658 - 3663
反应条件
1: trichoderin B With hydrogenchloride in water T=110°C; 20 h; 2: dabsyl chloride With sodium hydrogencarbonate in acetonitrile pH=8.1;
参考文献
Pruksakorn, Patamaporn; Arai, Masayoshi; Kotoku, Naoyuki; Vilchze, Catherine; Baughn, Anthony D.; Moodley, Prashini; Jacobs Jr., William R.; Kobayashi, Motomasa
Bioorganic and Medicinal Chemistry Letters, 2010 , vol. 20, # 12 p. 3658 - 3663
反应条件
sodium hydrogencarbonate in acetonitrile pH=8.1;
参考文献
Pruksakorn, Patamaporn; Arai, Masayoshi; Kotoku, Naoyuki; Vilchze, Catherine; Baughn, Anthony D.; Moodley, Prashini; Jacobs Jr., William R.; Kobayashi, Motomasa
Bioorganic and Medicinal Chemistry Letters, 2010 , vol. 20, # 12 p. 3658 - 3663
反应条件
hydrazine hydrate in tetrahydrofuran 0.5 h; Ambient temperature;
参考文献
Lin; Wu
Analytical Chemistry, 1987 , vol. 59, # 9 p. 1320 - 1326
反应条件
triethylamine in acetonitrile
T=20°C; 12 h;
参考文献
Industry-Academic Cooperation Foundation Yonsei University
Patent: US2009/270590 A1, 2009 ;
Location in patent: Page/Page column 19; 20 ;
反应条件
pyridine
Behandeln des Reaktionsprodukts mit Na2S2O4 in wss. NaOH;
参考文献
CIBA
Patent: CH210778 , 1938 ;
