9-苯基-8-氧杂-10-硫杂双环[4.4.0]癸-1,3,5-三烯-7-酮合成路线 （共 16 条）
反应条件
1: dihydrogen peroxide; methyltrioxorhenium (VII) / dichloromethane; water / 0.5 h / 20 °C 2: ammonia / toluene / 3 h / 50 °C View Scheme
参考文献
Shimizu, Masao; Shimazaki, Teruaki; Yoshida, Tetsuya; Ando, Wataru; Konakahara, Takeo
Tetrahedron, 2012 , vol. 68, # 21 p. 3932 - 3936
反应条件
Lawesson's reagent in benzene 16 h; Heating;
参考文献
El-Barbary, A. A.; Clausen, K.; Lawesson, S.-O.
Tetrahedron, 1980 , vol. 36, p. 3309 - 3316
反应条件
1: 89 percent / benzene / 1.3 h / Heating 2: 72 percent / 2,4-bis(4-methoxyphenyl)-1,3,2,4-dithiadiphosphetane-2,4-disulfide / hexamethylphosphoric acid triamide / 100 °C View Scheme
参考文献
El-Barbary, A. A.; Clausen, K.; Lawesson, S.-O.
Tetrahedron, 1980 , vol. 36, p. 3309 - 3316
反应条件
tetraphosphorus decasulfide in toluene 9 h; Heating;
参考文献
El-Barbary, A. A.; Hammouda, H. A.; El-Borai, M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 8 p. 770 - 773
反应条件
in toluene 6 h; Heating;
参考文献
El-Barbary, A. A.; Hammouda, H. A.; El-Borai, M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 8 p. 770 - 773
反应条件
potassium hydroxide 1) EtOH, H2O, 80 deg C - 90 deg C, 2) EtOH, H2O, 1 h, 80 deg C; Yield given. Multistep reaction;
参考文献
Chemische Berichte, , vol. 116, # 5 p. 1708 - 1727
反应条件
in benzene 9 h; Heating;
参考文献
El-Barbary, A. A.; Hammouda, H. A.; El-Borai, M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 8 p. 770 - 773
反应条件
in benzene 9 h; Heating;
参考文献
El-Barbary, A. A.; Hammouda, H. A.; El-Borai, M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 8 p. 770 - 773
反应条件
hydrazine in benzene 24 h; Heating;
参考文献
El-Barbary, A. A.; Clausen, K.; Lawesson, S.-O.
Tetrahedron, 1980 , vol. 36, p. 3309 - 3316
反应条件
sulfuric acid; acetic acid
T=105°C; P=20 - 30 Torr;
参考文献
Mowry
Journal of the American Chemical Society, 1947 , vol. 69, p. 2362
