(2E)-3-环己基-2-丙烯酸合成路线 (共 13 条)
反应条件
lithium hydroxide in tetrahydrofuran; water T=60°C; 12 h;
参考文献
Alhamadsheh, Mamoun M.; Palaniappan, Nadaraj; DasChouduri, Suparna; Reynolds, Kevin A.
Journal of the American Chemical Society, 2007 , vol. 129, # 7 p. 1910 - 1911
反应条件
pyrrolidine; pyridine T=20 - 60°C; 24 h;
参考文献
Smejkal, Tomas; Breit, Bernhard
Angewandte Chemie - International Edition, 2008 , vol. 47, # 21 p. 3946 - 3949
反应条件
samarium diiodide in tetrahydrofuran T=20°C; 2 h;
参考文献
Concellon, Jose M.; Concellon, Carmen
Journal of Organic Chemistry, 2006 , vol. 71, # 4 p. 1728 - 1731
反应条件
1: diethyl carboxymethylphosphonate With sodium hydride in ethylene glycol dimethyl ether T=20°C; 2: cyclohexanecarbaldehyde in ethylene glycol dimethyl ether T=20°C; Further stages.;
参考文献
Journal of the American Chemical Society, , vol. 129, # 26 p. 8064 - 8065
反应条件
1.1: NaH / 1,2-dimethoxy-ethane / 0 - 20 °C 1.2: 85 percent / 1,2-dimethoxy-ethane / 4 h 2.1: 91 percent / LiOH*H2O / tetrahydrofuran; H2O / 12 h / 60 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 129, # 7 p. 1910 - 1911
反应条件
1: With lithium hydroxide hydrate in tetrahydrofuran; water T=70°C; 15 h; 2: With hydrogenchloride in tetrahydrofuran; water T=0°C; pH=1 - 2; Overall yield = 1.48 g;
参考文献
Organic Letters, , vol. 14, # 17 p. 4610 - 4613
反应条件
lithium chloride; palladium dichloride in tetrahydrofuran; water T=-78°C;
参考文献
Journal of Organic Chemistry, , vol. 40, # 22 p. 3237 - 3242
反应条件
benzophenone 2.5 h; Irradiation; Title compound not separated from byproducts;
参考文献
Organic and Biomolecular Chemistry, , vol. 4, # 5 p. 942 - 952
反应条件
ethanol; silver(l) oxide
参考文献
Zhurnal Obshchei Khimii, , vol. 4, p. 866,867
Chem. Zentralbl., , vol. 106, # II p. 3766
反应条件
Yield given. Multistep reaction;
参考文献
Synthesis, , # 9 p. 690 - 691