2,2,3,3,4,4,5,5,6,6-十氟-1-(五氟乙基)哌啶合成路线 (共 11 条)
反应条件
hydrogen fluoride
T=7 - 8°C; 8.93333 h; electrochemical fluorination; Further byproducts given;
参考文献
Abe, Takashi; Hayashi, Eiji; Fukaya, Haruhiko; Hayakawa, Yoshio; Baba, Hajime; et al.
Journal of Fluorine Chemistry, 1992 , vol. 57, p. 101 - 111
反应条件
hydrogen fluoride
T=7 - 8°C; 9.15 h; electrochemical reaction; anodic current density of 3.5 A dm-2, a cell voltage of 6.1 V - 6.3 V; Further byproducts given;
参考文献
Abe, Takashi; Fukaya, Haruhiko; Hayashi, Eiji; Hayakawa, Yoshio; Nishida, Masakazu; Baba, Hajime
Journal of Fluorine Chemistry, 1994 , vol. 66, # 2 p. 193 - 202
反应条件
hydrogen fluoride
T=7 - 8°C; 8.55 h; electrochemical reaction; anodic current density of 3.5 A dm-2, a cell voltage of 6.1 V - 6.3 V; Further byproducts given;
参考文献
Abe, Takashi; Fukaya, Haruhiko; Hayashi, Eiji; Hayakawa, Yoshio; Nishida, Masakazu; Baba, Hajime
Journal of Fluorine Chemistry, 1994 , vol. 66, # 2 p. 193 - 202
反应条件
hydrogen fluoride
T=7 - 8°C; 8.93333 h; electrochemical fluorination; Yield given. Further byproducts given. Title compound not separated from byproducts;
参考文献
Abe, Takashi; Hayashi, Eiji; Fukaya, Haruhiko; Hayakawa, Yoshio; Baba, Hajime; et al.
Journal of Fluorine Chemistry, 1992 , vol. 57, p. 101 - 111
反应条件
hydrogen fluoride
T=7 - 8°C; 8.93333 h; electrochemical fluorination; Yield given. Further byproducts given. Title compound not separated from byproducts;
参考文献
Abe, Takashi; Hayashi, Eiji; Fukaya, Haruhiko; Hayakawa, Yoshio; Baba, Hajime; et al.
Journal of Fluorine Chemistry, 1992 , vol. 57, p. 101 - 111
反应条件
hydrogen fluoride
T=7 - 8°C; 8.93333 h; electrochemical fluorination; Yield given. Further byproducts given. Title compound not separated from byproducts;
参考文献
Abe, Takashi; Hayashi, Eiji; Fukaya, Haruhiko; Hayakawa, Yoshio; Baba, Hajime; et al.
Journal of Fluorine Chemistry, 1992 , vol. 57, p. 101 - 111
反应条件
hydrogen fluoride
T=7 - 8°C; 9.15 h; electrochemical reaction; anodic current density of 3.5 A dm-2, a cell voltage of 6.1 V - 6.3 V; Further byproducts given;
参考文献
Abe, Takashi; Fukaya, Haruhiko; Hayashi, Eiji; Hayakawa, Yoshio; Nishida, Masakazu; Baba, Hajime
Journal of Fluorine Chemistry, 1994 , vol. 66, # 2 p. 193 - 202
反应条件
hydrogen fluoride
electrochemical fluorination, 253 Ahr;
参考文献
Abe, Takashi; Hayashi, Eiji; Fukaya, Haruhiko; Baba, Hajime
Journal of Fluorine Chemistry, 1990 , vol. 50, # 2 p. 173 - 196
反应条件
hydrogen fluoride
T=8 - 12°C; 5.58333 h; electrochemical fluorination: nickel electrodes, anodic current density: 4.0 A/dm2, cell voltage 5.6 - 6.7 V;
参考文献
Hayashi, Eiji; Abe, Takashi; Baba, Hajime; Nagase, Shunji
Journal of Fluorine Chemistry, 1983 , vol. 23, p. 371 - 382
反应条件
hydrogen fluoride
T=7 - 8°C; 9.15 h; electrochemical reaction; anodic current density of 3.5 A dm-2, a cell voltage of 6.1 V - 6.3 V; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Abe, Takashi; Fukaya, Haruhiko; Hayashi, Eiji; Hayakawa, Yoshio; Nishida, Masakazu; Baba, Hajime
Journal of Fluorine Chemistry, 1994 , vol. 66, # 2 p. 193 - 202