5,10,15,20-四(2,4,6-三甲苯基)-21H,23H-卟吩合成路线 （共 15 条）
反应条件
1: CF3SO2Cl / CH2Cl2 / 1 h / 20 °C 2: air / CH2Cl2 / 4 h / 39 °C View Scheme
参考文献
Tetrahedron, , vol. 60, # 8 p. 1863 - 1868
反应条件
hydrochloride acetic acid T=0°C; 0.0166667 h;
参考文献
Journal of the American Chemical Society, , vol. 108, # 24 p. 7836 - 7837
反应条件
1: With boron trifluoride diethyl etherate in chloroform T=20°C; Lindsey reaction; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in chloroform 1 h;
参考文献
Chang, Christopher J.; Yeh, Chen-Yu; Nocera, Daniel G.
Journal of Organic Chemistry, 2002 , vol. 67, # 4 p. 1403 - 1406
反应条件
titanium tetrachloride in dichloromethane 1 h; Ambient temperatureother reagents: VOCl3, VO(OEt)Cl2, VO(OiPr)Cl2, Mn(OAc)3;
参考文献
Gradillas, Ana; Campo, Carmen del; Sinisterra, Jose V.; Llama, Emilio F.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 20 p. 2611 - 2614
反应条件
1: With boron trifluoride diethyl etherate in chloroform T=20°C; 1.5 h; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in chloroform 0.25 h;
参考文献
Lewtak, Jan P.; Gryko, Dorota; Bao, Duoduo; Sebai, Ernest; Vakuliuk, Olena; Scigaj, Mateusz; Gryko, Daniel T.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 23 p. 8178 - 8181
反应条件
1: With boron trifluoride diethyl etherate in chloroform 1 h; DarknessInert atmosphere; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in chloroform 1 h;
参考文献
Organic Letters, , vol. 12, # 5 p. 1036 - 1039
反应条件
1: With boron trifluoride diethyl etherate in chloroform T=20°C; 1 h; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in chloroform T=20°C; 1 h; Further stages. Title compound not separated from byproducts.;
参考文献
Journal of Organic Chemistry, , vol. 72, # 14 p. 5207 - 5217
反应条件
1: With boron trifluoride diethyl etherate in dichloromethane T=20°C; 0.5 h; Inert atmosphereDarkness; 2: With triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane 1 h; Inert atmosphereDarkness;
参考文献
Journal of Porphyrins and Phthalocyanines, , vol. 14, # 6 p. 469 - 480
反应条件
boron trifluoride diethyl etherate; 2,3-dicyano-5,6-dichloro-p-benzoquinone 1.) CHCl3, RT, 2.) CHCl3, RT; Yield given. Multistep reaction. Further byproducts given;
参考文献
Journal of the American Chemical Society, , vol. 118, # 45 p. 11166 - 11180
反应条件
boron trifluoride diethyl etherate; 2,3-dicyano-5,6-dichloro-p-benzoquinone 1.) CHCl3, RT, 1 h, 2.) CHCl3, RT, 1 h; Yield given. Multistep reaction. Further byproducts given;
参考文献
Journal of the American Chemical Society, , vol. 118, # 45 p. 11166 - 11180
