5-异丙基-1H-吡唑-3-胺合成路线 （共 2 条）
反应条件
hydrazine in ethanol 1 h; Heating / reflux;
参考文献
BRISTOL-MYERS SQUIBB COMPANY; PURANDARE, Ashok V.; FRENNESSON, David B.; KAMAU, Muthoni G.; HARIKRISHNAN, Lalgudi S.; SAULNIER, Mark G.
Patent: WO2010/42684 A1, 2010 ;
Location in patent: Page/Page column 58 ;
WO 2010/042684 A1
反应条件
1: hydrazine hydrate / CH2Cl2 / 14 h / Heating 2: 3-enenitrile (5a) / 0.33 h / 80 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2997 - 3001
