苄基 4,6-O-亚苄基-beta-D-吡喃半乳糖苷合成路线 （共 9 条）
反应条件
indium trifluoromethanesulfonate T=30°C; 0.0333333 h;
参考文献
Giri, Santosh Kumar; Verma, Monika; Kartha, K. P. Ravindranathan
Journal of Carbohydrate Chemistry, 2008 , vol. 27, # 8-9 p. 464 - 478
反应条件
camphor-10-sulfonic acid in N,N-dimethyl-formamide T=80°C; 16 h; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 60, # 8 p. 2570 - 2580
反应条件
1: 12.4 g / NaOMe; MeOH / 2 h 2: 12.4 g / CSA / CHCl3 / 1 h / Heating View Scheme
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 5 p. 543 - 551
反应条件
1: BF3*Et2O / CH2Cl2 / 12 h / 20 °C 2: 12.4 g / NaOMe; MeOH / 2 h 3: 12.4 g / CSA / CHCl3 / 1 h / Heating View Scheme
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 5 p. 543 - 551
反应条件
1: BF3*Et2O / CH2Cl2 / 12 h / 20 °C 2: 12.4 g / NaOMe; MeOH / 2 h 3: 12.4 g / CSA / CHCl3 / 1 h / Heating View Scheme
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 5 p. 543 - 551
反应条件
1: HCl / 4 h / 80 - 100 °C 2: ZnCl2 / 4 h / Ambient temperature View Scheme
参考文献
Carbohydrate Research, , vol. 253, # 1 p. 167 - 184
反应条件
zinc(II) chloride 4 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Carbohydrate Research, , vol. 253, # 1 p. 167 - 184
反应条件
sodium hydride 1.) 24 deg C, 30 min, 2.) 24 deg C, 1 h;
参考文献
Kobayashi; Shiozaki; Ando
Journal of Organic Chemistry, 1995 , vol. 60, # 8 p. 2570 - 2580
反应条件
1.1: NaH / dimethylformamide / 0.5 h / 20 °C 1.2: 16.8 g / Bu4NI / dimethylformamide 2.1: 13.6 g / PTSA; propane-1,3-diol / CH2Cl2; methanol / 96 h / Heating View Scheme
参考文献
Clausen, Mads H.; Jorgensen, Malene R.; Thorsen, Jesper; Madsen, Robert
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 5 p. 543 - 551
