1-甲氧基-4-(苯硫基)-苯合成路线 (共 118 条)
反应条件
potassium tert-butylate in dimethyl sulfoxide
T=40 - 80°C; Overall yield = 81 percent; Overall yield = 0.17 g;
参考文献
Kumar, Sangit; Kumar, Amit; Bhakuni, Bhagat Singh; Prasad, Ch. Durga; Kumar, Shailesh
Tetrahedron, 2013 , vol. 69, # 26 p. 5383 - 5392
反应条件
copper in neat (no solvent)
T=200°C; 1 h;
参考文献
Akutagawa, Kunihiko; Furukawa, Naomichi; Oae, Shigeru
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 19, p. 213 - 222
反应条件
4-MeC6H4SNa in N,N-dimethyl-formamide
T=26°C; 77 h; Irradiation;
参考文献
Fujimori, K.; Togo, H.; Pelchers, Y.; Nagata, T.; Furukawa, N.; Oae, S.
Tetrahedron Letters, 1985 , vol. 26, # 6 p. 775 - 778
反应条件
iodine; magnesium in methanol
T=20°C; 3 h;
参考文献
Khurana, Jitender M.; Sharma, Vandana; Chacko, Silvi A.
Tetrahedron, 2007 , vol. 63, # 4 p. 966 - 969
反应条件
o-phenylene-bislt;diphenylphosphinogt;-nickel(II) bromide in ethylene glycol
T=200°C; 24 h;
参考文献
Cristau, H. J.; Chabaud, B.; Chene, A.; Christol, H.
Synthesis, 1981 , # 11 p. 892 - 894
反应条件
copper(l) iodide; [DBU][HOAc]
T=130°C; 0.166667 h; Microwave irradiation;
参考文献
Singh, Neetu; Singh, Rahul; Raghuvanshi, Dushyant S.; Singh, Krishna Nand
Organic Letters, 2013 , vol. 15, # 22 p. 5874 - 5877
反应条件
copper(l) iodide; [DBU][HOAc]
T=130°C; 0.166667 h; Microwave irradiation;
参考文献
Singh, Neetu; Singh, Rahul; Raghuvanshi, Dushyant S.; Singh, Krishna Nand
Organic Letters, 2013 , vol. 15, # 22 p. 5874 - 5877
反应条件
sulfuric acid in trifluoroacetic acid
T=25°C; 2 h;
参考文献
Takeuchi, Hiroshi; Hiyama, Takehiro; Kamai, Noriyoshi; Oya, Hiromi
Journal of the Chemical Society. Perkin Transactions 2, 1997 , # 11 p. 2301 - 2305
反应条件
tert.-butylnitrite; C29H23N6Ru2(2+)*2Cl(1-)*6H2O; toluene-4-sulfonic acid in acetonitrile
T=20°C; 5 h; Irradiation;
参考文献
Wang, Xiao; Cuny, Gregory D.; Noel, Timothy
Angewandte Chemie - International Edition, 2013 , vol. 52, # 30 p. 7860 - 7864
Angew. Chem., 2013 , vol. 125, # 30 p. 8014 - 8018,5
反应条件
copper(l) iodide; [DBU][HOAc]
T=130°C; 0.166667 h; Microwave irradiation;
参考文献
Singh, Neetu; Singh, Rahul; Raghuvanshi, Dushyant S.; Singh, Krishna Nand
Organic Letters, 2013 , vol. 15, # 22 p. 5874 - 5877