2-(2-氯乙氧基)四氢-2H-吡喃合成路线 (共 16 条)
反应条件
Envirocat EPZG T=0 - 5°C; 0.25 h;
参考文献
Bandgar; Jagtap; Aghade; Wadgaonkar
Synthetic Communications, 1995 , vol. 25, # 15 p. 2211 - 2215
参考文献
Ranu, Brindaban C.; Hajra, Alakananda
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 4 p. 355 - 357
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Ranu, Brindaban C.; Hajra, Alakananda
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 18 p. 2262 - 2265
反应条件
(i) LiNEt2, HMPT, benzene, (ii) K, HMPT, tBuOH, (iii) TsOH; Multistep reaction;
参考文献
Debal,A. et al.
Synthesis, 1976 , p. 391 - 393
反应条件
hydrogenchloride; potassium hydroxide; tetrabutyl-ammonium chloride in ethanol; toluene
参考文献
Schering Aktiengesellschaft
Patent: US6083479 A1, 2000 ;
反应条件
sulfuric acid; silica gel in methanol T=20°C; 0.5 h;
参考文献
Hajipour, Abdol R.; Zarei, Amin; Khazdooz, Leila; Pourmousavi, Seied A.; Zahmatkesh, Saeed; Ruoho, Arnold E.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 1 p. 305 - 308
反应条件
methanol; DOWEX 50 W-X2 cation exchange resin T=40°C; 1.33333 h;
参考文献
Tanacs, B.; Kling, F.; Mucha, I.; Marton, J.
Acta Chimica Hungarica, 1983 , vol. 112, # 2 p. 233 - 240
反应条件
methanol; DOWEX 50 W-X2 cation exchange resin T=40°C; 1.33333 h;
参考文献
Tanacs, B.; Kling, F.; Mucha, I.; Marton, J.
Acta Chimica Hungarica, 1983 , vol. 112, # 2 p. 233 - 240
反应条件
in concentrated aqueous hydrochloric acid; ethanol
参考文献
Boehringer Ingelheim Pharmaceuticals, Inc.
Patent: US5571809 A1, 1996 ;
反应条件
potassium hydroxide 1) DMSO, 5 min, 2) r.t., overnight; Yield given. Multistep reaction;
参考文献
Zeitschrift fuer Naturforschung, B: Chemical Sciences, , vol. 44, # 8 p. 983 - 987
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate T=65°C; 72 h;
参考文献
Gibson, Harry W.; Bheda, Mukesh C.; Engen, Paul; Shen, Ya Xi; Sze, Jean; et al.
Journal of Organic Chemistry, 1994 , vol. 59, # 8 p. 2186 - 2196