2,3-二甲基-2-丁烯合成路线 （共 833 条）
参考文献
Closs,G.L.; Coyle,J.J.
Journal of the American Chemical Society, 1965 , vol. 87, p. 4270 - 4279
反应条件
in dichloromethane
Irradiation;
参考文献
Yang,N.C.; Marolewski,T.A.
Journal of the American Chemical Society, 1968 , vol. 90, p. 5644 - 5646
反应条件
1: zinc/copper couple / diethyl ether / 19 h / Inert atmosphere; Reflux
2: zinc/copper couple; ammonium chloride / methanol / 4 h / 20 - 45 °C / Inert atmosphere
View Scheme
参考文献
Okuno, Ryosuke; Matsuo, Jun-Ichi; Ishibashi, Hiroyuki
Chemical and Pharmaceutical Bulletin, 2012 , vol. 60, # 6 p. 793 - 797
反应条件
oxygen in benzene
20 h; Irradiation;
参考文献
Machida, Minoru; Oda, Kazuaki; Kanaoka, Yuichi
Tetrahedron Letters, 1984 , vol. 25, # 4 p. 409 - 410
反应条件
GLC-SbF5
T=70°C; 1 h;
参考文献
Kvacheva, L. D.; Klimakhina, S. T.; Grigor'eva, L. T.; Podberezina, A. S.; Novikov, Yu. N.; et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 1741 - 1743
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 8 p. 1907 - 1909
参考文献
Ramos, Susana S.; Almeida, Paulo; Santos, Lina; Motherwell, William B.; Sheppard, Tom D.; Costa, Maria do Ceu
Tetrahedron, 2007 , vol. 63, # 51 p. 12608 - 12615
反应条件
tin(IV) chloride
T=0°C;
参考文献
Dubois, Jacques-Emile; Saumtally, Imran; Lion, Claude
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 3-4 p. 133 - 138
反应条件
lithium azide; oxygen; rose bengal in methanol
T=30°C; 48 h; Irradiation; Title compound not separated from byproducts;
参考文献
Griesbeck, Axel G.; Hundertmark, Thomas; Steinwascher, Joerg
Tetrahedron Letters, 1996 , vol. 37, # 46 p. 8367 - 8370
反应条件
sodium azide; oxygen; 9-(2-carboxyphenyl)-3,6-bis(diethylamino)xanthylium chloride; sodium sulfite
1.) MeOH/H2O, irradiation, 30 deg C, 24 h; 2.) MeOH/H2O; Yield given. Multistep reaction;
参考文献
Griesbeck, Axel G.; Hundertmark, Thomas; Steinwascher, Joerg
Tetrahedron Letters, 1996 , vol. 37, # 46 p. 8367 - 8370
反应条件
benzophenone; lithium azide; oxygen in methanol
T=30°C; 48 h; Irradiationphotooxygenation of various alkenes; Product distributionMechanism;
参考文献
Griesbeck, Axel G.; Hundertmark, Thomas; Steinwascher, Joerg
Tetrahedron Letters, 1996 , vol. 37, # 46 p. 8367 - 8370
