in water Tl2CO3 dissolved in a slight excess aq. CH3COOH;; evapn. to dryness on a water bath; residue molten on a sand bath until odour of CH3COOH is gone, dissolved in H2O; soln. filtrated, evapd.; crystn.;;
参考文献
Chem. News J. Ind. Sci., , vol. 8, p. 279 - 279
Journal of the Chemical Society, , vol. 17, p. 149 - 149
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 30, p. 1781 - 1781
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 2166 - 2166
in toluene addn. of TlC5Me5 to a soln. of (Cl(PMe3)Pd)2(CH3CO2)2 in toluene and stirring at room temp. for 6 h (N2); addn. of hexane to the reaction mixt., filtn. and cooling the filtrate to -78°C, formation of dark green crystals after a few days, washing the crystals with cold pentane and drying in vacuo, elem. anal.;
参考文献
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, , vol. 38, # 6 p. 733 - 737
in toluene addn. of TlC5Me5 to a soln. of (Cl(P(i-Pr)3)Pd)2(CH3CO2)2 in toluene and stirring at room temp. for 6 h (N2); addn. of hexane to the reaction mixt., filtn. and cooling the filtrate to -78°C, formation of dark green crystals after a few days, washing the crystals with cold pentane and drying in vacuo, elem. anal.;
参考文献
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, , vol. 38, # 6 p. 733 - 737
