[1R-(1alpha,2alpha,5alpha)]-6,6-二甲基螺[双环[3.1.1]庚烷-2,2'-环氧乙烷]合成路线 （共 7 条）
反应条件
1: acetic acid / auf Siedetemperatur erhitzen und Erhitzen des Reaktionsprodukts bis auf 240grad 2: ethanolic NaOH-solution 3: CrO3; acetic acid; water View Scheme
参考文献
Kergomard; Philibert-Bigou
Bulletin de la Societe Chimique de France, 1958 , p. 393
反应条件
1: With bis(cyclopentadienyl)titanium dichloride; zinc in tetrahydrofuran T=20°C; Inert atmosphere; 2: With sodium dihydrogenphosphate in tetrahydrofuran Inert atmosphere;
参考文献
Fernandez-Mateos; Herrero Teijon; Rubio Gonzalez
Tetrahedron, 2011 , vol. 67, # 49 p. 9529 - 9534
反应条件
carbon dioxide; water 4 h;
参考文献
Ohloff; Giersch
Helvetica Chimica Acta, 1980 , vol. 63, # 1 p. 76 - 94
反应条件
niobium pentachloride in ethyl acetate T=20°C; 0.0166667 h; Title compound not separated from byproducts.;
参考文献
Constantino, Mauricio Gomes; Lacerda Jr., Valdemar; Invernize, Paulo Roberto; Filho, Luiz Carlos Da Silva; Da Silva, Gil Valdo Jose
Synthetic Communications, 2007 , vol. 37, # 20 p. 3529 - 3539
反应条件
hydrogen fluoride; triethylamine
参考文献
Kergomard; Philibert-Bigou
Bulletin de la Societe Chimique de France, 1958 , p. 393
反应条件
lithium aluminium tetrahydride; diethylamine in diethyl ether
参考文献
Farges,G.; Kergomard,A.
Bulletin de la Societe Chimique de France, 1975 , p. 315 - 318
参考文献
Kergomard; Philibert
Bulletin de la Societe Chimique de France, 1959 , p. 1381,1384
