(3-氯苯基)(2-甲基苯基)甲酮合成路线 (共 4 条)
反应条件
1: 2-methylphenylmagnesium chloride With zinc(II) chloride in 1-methyl-pyrrolidin-2-one; diethyl ether
T=60°C; 0.333333 h;
2: meta-chlorobenzoyl chloride With ((t-Bu)2POH)2PdCl2 in 1-methyl-pyrrolidin-2-one
T=25°C; 0.5 h; Further stages.;
参考文献
Xu, Hanhui; Ekoue-Kovi, Kekeli; Wolf, Christian
Journal of Organic Chemistry, 2008 , vol. 73, # 19 p. 7638 - 7650
反应条件
in tetrahydrofuran
T=-15 - 0°C; 3 h;
参考文献
Lee, Jae In
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 3 p. 749 - 752
反应条件
palladium diacetate in diethyl ether; acetonitrile
2 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Kikukawa, Kiyoshi; Idemoto, Tohru; Katayama, Atsuhiko; Kono, Kiyoshi; Wada, Fumio; Matsuda, Tsutomu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1511 - 1514
反应条件
sulfonic acid catalyst
参考文献
Olah,G.A. et al.
Synthesis, 1978 , p. 672 - 673