2-(BOC- 氨基)-5-甲基吡啶合成路线 (共 2 条)
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane 1.5 h; Reflux;
参考文献
AVENTIS PHARMA DEUTSCHLAND GMBH
Patent: WO2005/105781 A1, 2005 ;
Location in patent: Page/Page column 49 ;
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane
T=20°C; 16 h; Inert atmosphere;
参考文献
NOVARTIS AG
Patent: WO2009/141386 A1, 2009 ;
Location in patent: Page/Page column 122-123 ;
WO 2009/141386 A1