N,N′,N′′-三(对甲苯磺酰)二乙撑三胺合成路线 （共 18 条）
反应条件
sodium hydroxide in diethyl ether; water T=0°C; 1 h;
参考文献
Wilson, Jennifer M.; Giordani, Federica; Farrugia, Louis J.; Barrett, Michael P.; Robins, David J.; Sutherland, Andrew
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 22 p. 3651 - 3656
反应条件
hydrogenchloride in pyridine; N,N-dimethyl-formamide
参考文献
Monsanto Company
Patent: US5610293 A1, 1997 ;
反应条件
triethylamine in dichloromethane T=-48 - 20°C; 8 h;
参考文献
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, , vol. 62, # 3 p. 397 - 406
反应条件
sodium hydroxide in water 1.) 5 deg C, 1 hr., 2.) 3 hrs., r.t.;
参考文献
Luk'yanenko, N.G.; Basok, S.S.; Filonova, L.K.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, p. 1562 - 1571
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 8 p. 1731 - 1742
反应条件
sodium in ethanol; N,N-dimethyl-formamide T=80°C;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 59, # 4 p. 1031 - 1036
参考文献
Journal of the Chemical Society, , p. 1519
反应条件
potassium carbonate in N,N-dimethyl-formamide 53 h; Ambient temperaturealso other reaction conditions; Product distribution;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 59, # 4 p. 1031 - 1036
反应条件
sodium hydroxide; tetra-(n-butyl)ammonium iodide in water; toluene 9 h; Heating;
参考文献
Luk'yanenko, N.G.; Basok, S.S.; Filonova, L.K.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, p. 1562 - 1571
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 8 p. 1731 - 1742
反应条件
caesium carbonate in acetonitrile T=80°C; 48 h;
参考文献
Kohl, Stephan W.; Kuse, Katharina; Hummert, Markus; Schumann, Herbert; Muegge, Clemens; Janek, Katharina; Weisshoff, Hardy
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2007 , vol. 62, # 3 p. 397 - 406
反应条件
1: 91 percent / sodium ethoxide / ethanol / 1 h / Heating 2: 67 percent / dimethylformamide / 1 h / Heating View Scheme
参考文献
Swinkels, Dorine W.; Duynhoven, John P. M. van; Hilbers, Cornelis W.; Tesser, Godefridus I.
Recueil des Travaux Chimiques des Pays-Bas, 1991 , vol. 110, # 4 p. 124 - 128
