3-甲基-2,5-二吡咯烷酮合成路线 （共 15 条）
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Blicke; Lu
Journal of the American Chemical Society, 1952 , vol. 74, p. 3993
反应条件
T=20 - 60°C; elektrolytische Reduktion;
参考文献
Spaeth; Breusch
Monatshefte fuer Chemie, 1928 , vol. 50, p. 352
Full Text Show Details
Spaeth; Prokopp
Chemische Berichte, 1924 , vol. 57, p. 478
反应条件
hydrogen; palladium on activated charcoal in ethanol
P=760 Torr;
参考文献
Kuehne, Paul; Hesse, Manfred
Tetrahedron, 1993 , vol. 49, # 21 p. 4575 - 4580
反应条件
(4,5-bis((diphenylphosphino)methyl)-2,2-dimethyl-1,3-dioxolane)palladium(II)Cl2 in methanol; benzene
T=120°C; P=154280 Torr; 40 h; Yield given. Yields of byproduct given;
参考文献
Consiglio, Giambattista; Kollar, Laszlo; Koelliker, Robert
Journal of Organometallic Chemistry, 1990 , vol. 396, # 2/3 p. 375 - 383
反应条件
(4,5-bis((diphenylphosphino)methyl)-2,2-dimethyl-1,3-dioxolane)palladium(II)Cl2 in benzene
T=120°C; P=154280 Torr; 40 h; Yields of byproduct given;
参考文献
Consiglio, Giambattista; Kollar, Laszlo; Koelliker, Robert
Journal of Organometallic Chemistry, 1990 , vol. 396, # 2/3 p. 375 - 383
反应条件
1: 51 percent / NH4OAc, AcOH / 2 h / Heating
2: 97 percent / H2 / 10percent Pd-C / ethanol / 760 Torr
View Scheme
参考文献
Kuehne, Paul; Hesse, Manfred
Tetrahedron, 1993 , vol. 49, # 21 p. 4575 - 4580
反应条件
bis(1,5-cyclooctadiene)nickel (0); tri-cyclo-hexyl-phosphine
1.) THF, 6 h, 2.) ether; Yield given. Multistep reaction;
参考文献
Yamamoto,T.; Igarishi,K.; Komiya,S.
Journal of the American Chemical Society, 1980 , vol. 102, p. 7448
反应条件
ammonium hydroxide
T=280°C;
参考文献
Menger, F.M.; Lee, L. H.
Tetrahedron Letters, 1988 , vol. 29, # 7 p. 757 - 760
反应条件
1: OH(1-)
2: NH4OH / 280 °C
View Scheme
参考文献
Menger, F.M.; Lee, L. H.
Tetrahedron Letters, 1988 , vol. 29, # 7 p. 757 - 760
参考文献
Spaeth; Prokopp
Chemische Berichte, 1924 , vol. 57, p. 478
