2-氯-4,5-二硝基甲苯合成路线 (共 11 条)
反应条件
1: alcohol; ammonia 2: tin (II)-chloride; alcohol View Scheme
参考文献
Morgan; Drew
Journal of the Chemical Society, 1920 , vol. 117, p. 789
参考文献
Morgan; Challenor
Journal of the Chemical Society, 1921 , vol. 119, p. 1540
Full Text Show Details
Morgan; Drew
Journal of the Chemical Society, 1920 , vol. 117, p. 789
反应条件
sulfuric acid; urea hydronitrate
T=0 - 20°C; Nitration;
参考文献
Mundla, Sreenivasa R.
Tetrahedron Letters, 2000 , vol. 41, # 22 p. 4277 - 4279
反应条件
sulfuric acid; nitric acid
T=40 - 45°C; dann bei 90grad; man trennt die isomeren Verbindungen durch fraktionierte Krystallisation aus konz. Schwefelsaeure;
参考文献
Morgan; Challenor
Journal of the Chemical Society, 1921 , vol. 119, p. 1540
Full Text Show Details
Morgan; Drew
Journal of the Chemical Society, 1920 , vol. 117, p. 789
反应条件
hydrogenchloride; copper(l) chloride
T=70°C; Diazotization;
参考文献
Morgan; Glover
Journal of the Chemical Society, 1921 , vol. 119, p. 1706
反应条件
sulfuric acid; nitric acid
T=8 - 10°C; man trennt die Isomeren durch aufeinanderfolgende fraktionierte Krystallisation aus konz. Schwefelsaeure und Alkohol;
参考文献
Morgan; Drew
Journal of the Chemical Society, 1920 , vol. 117, p. 789
参考文献
Morgan; Drew
Journal of the Chemical Society, 1920 , vol. 117, p. 789
参考文献
Morgan; Challenor
Journal of the Chemical Society, 1921 , vol. 119, p. 1540
Show Details
Morgan; Drew
Journal of the Chemical Society, 1920 , vol. 117, p. 789
参考文献
Morgan; Challenor
Journal of the Chemical Society, 1921 , vol. 119, p. 1540
Show Details
Morgan; Drew
Journal of the Chemical Society, 1920 , vol. 117, p. 789
反应条件
1: alcohol; ammonia
2: Diazotization.folgend Behandeln mit Kupfer(I)-chlorid in Salzsaeure
View Scheme
参考文献
Morgan; Drew
Journal of the Chemical Society, 1920 , vol. 117, p. 789