(Z)-3-(亚异丁基)苯酞合成路线 （共 5 条）
反应条件
triethylamine; palladium diacetate; 1,3-bis-(diphenylphosphino)propane in N,N-dimethyl-formamide
T=60°C; 1 h;
参考文献
Ciattini; Mastropietro; Morera; Ortar
Tetrahedron Letters, 1993 , vol. 34, # 23 p. 3763 - 3766
反应条件
sodium acetate in ethanol
3 h; Heating;
参考文献
Mali; Patil; Kulkarni; Yeola
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 4 p. 319 - 321
反应条件
1: 90 percent / I2, aq. KI, aq. NaHCO3 / 0.5 h
2: 55 percent / NaOAc / ethanol / 3 h / Heating
View Scheme
参考文献
Mali; Patil; Kulkarni; Yeola
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 4 p. 319 - 321
反应条件
1: 1) potassium t-butoxide / 1.) t-butanol, ether, 20 min, 2.) THF, 2 h
2: 90 percent / I2, aq. KI, aq. NaHCO3 / 0.5 h
3: 55 percent / NaOAc / ethanol / 3 h / Heating
View Scheme
参考文献
Mali; Patil; Kulkarni; Yeola
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 4 p. 319 - 321
反应条件
lithium hexamethyldisilazane
1.) THF, hexane, -78 deg C, 1 h, 2.) THF, hexane, -78 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Watanabe, Mitsuaki; Ijichi, Saori; Morimoto, Hitoshi; Nogami, Kayoko; Furukawa, Sunao
Heterocycles, 1993 , vol. 36, # 3 p. 553 - 563
