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sodium tetrahydroborate; sodium carbonate in water T=20°C; 1 h; chemoselective reaction;

sodium hydrogencarbonate; trifluoroacetic acid

C10H16NO5; potassium carbonate; bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane T=-15°C; 4 h; chemoselective reaction;

T=180 - 190°C;

toluene Verseifen das erhaltenen Acetat mit Kalilauge;

暂无反应条件数据

1: 1.) TosCl; 2.) LiCl / 1.) pyridine; 2.) DMF 2: 72 percent / titanium tetrachloride / diethyl ether 3: 83 percent / potassium t-butoxide / tetrahydrofuran / 2 h / Heating 4: 82 percent / aq. oxalic acid / Ambient temperature 5: CH2Cl2 / Ambient temperature 6: RuO2, NaIO4 / acetone; H2O 7: H3O(1+) / H2O / 6 h / Heating View Scheme

P2O5; benzene T=230°C;

暂无反应条件数据