1,3-二苯基-1,1,3,3-四甲基二硅氧合成路线 (共 106 条)
反应条件
1 Au/TiO2; water in ethyl acetate T=25°C; 0.5 h; Reagent/catalyst;
参考文献
Gryparis, Charis; Stratakis, Manolis
Chemical Communications (Cambridge, United Kingdom), 2012 , vol. 48, # 87 p. 10751 - 10753,3
反应条件
[{Rh(μ-Cl)(1,5-cyclooctadiene)}2]; water in dichloromethane 12 h; Ambient temperature;
参考文献
Shi, Min; Nicholas, Kenneth M.
Journal of Chemical Research - Part S, 1997 , # 11 p. 400 - 401
反应条件
18-crown-6 ether; water; cesium fluoride in toluene T=50°C; 20 h;
参考文献
Journal of Organometallic Chemistry, , vol. 686, # 1-2 p. 52 - 57
反应条件
oxygen; palladium diacetate; 1,3-bis-(diphenylphosphino)propane in dimethyl sulfoxide T=50°C; 24 h;
参考文献
Yoshida, Hiroto; Yamaryo, Yasuhito; Ohshita, Joji; Kunai, Atsutaka
Chemical Communications, 2003 , # 13 p. 1510 - 1511
反应条件
2,6-di-tert-butyl-pyridine; trimethylsilyl trifluoromethanesulfonate in dichloromethane T=-78 - 20°C; 24 h;
参考文献
Synlett, , # 12 p. 1909 - 1912
反应条件
hydrogen fluoride in acetonitrile
参考文献
Magar, Sharad S.; Fuchs, P. L.
Tetrahedron Letters, 1991 , vol. 32, # 51 p. 7513 - 7516
反应条件
1: (Me2PhSi)3CH With methyllithium in tetrahydrofuran Peterson olefination; 2 h; Inert atmosphereReflux; 2: formaldehyd in tetrahydrofuran T=20°C; Peterson olefination; 12 h; Inert atmosphere;
参考文献
Izod, Keith; Bowman, Lyndsey J.; Wills, Corinne; Clegg, William; Harrington, Ross W.
Dalton Transactions, 2009 , # 17 p. 3340 - 3347
反应条件
scandium tris(trifluoromethanesulfonate) in acetonitrile T=0°C; 1 h;
参考文献
Hreczycho, Grzegorz; Pawluc, Piotr; Marciniec, Bogdan
New Journal of Chemistry, 2011 , vol. 35, # 12 p. 2743 - 2746
反应条件
scandium tris(trifluoromethanesulfonate) in acetonitrile T=0°C; 1 h;
参考文献
Hreczycho, Grzegorz; Pawluc, Piotr; Marciniec, Bogdan
New Journal of Chemistry, 2011 , vol. 35, # 12 p. 2743 - 2746
反应条件
2,6-di-tert-butyl-pyridine; trimethylsilyl trifluoromethanesulfonate in dichloromethane T=-78 - 20°C; Prins reaction; 4 h;
参考文献
Synlett, , # 12 p. 1909 - 1912