Goryushkin, V. F.; Zalymova, S. A.; Poshevneva, A. I.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1990 , vol. 35, p. 1749 - 1752
Zhurnal Neorganicheskoi Khimii, 1990 , vol. 35, p. 3081 - 3085
in neat (no solvent) calcination of purified ZrO2 in CCl4/Cl2 at 550-600°C in a porcelain tube, covered with asbestos, in iron tube; precipitation of the product at the colder part of the tube;; sublimation of ZrCl4 in a slow stream of gas at 140°C;;
参考文献
Journal of the Chemical Society, , vol. 125, p. 1252 - 1261
in gaseous matrix Irradiation (UV/VIS); metal atoms produced by laser ablation with a Nd:YAG laser, co-depositedwith CCl4 in Ar onto a CsI window cooled to 8 K, irradiated with UV; not isolated, detected by IR;
