in neat (no solvent) on passing CCl4 at 900°C and 0.05-0.1 Torr with 10 m/s through a quartz tube;; determination by IR at -190°C; molar ratio C2Cl6:C2Cl4=10:1;;
in neat (no solvent) reaction of ZnH2 with CCl4 at 20-250°C; below the b.p. of CCl4 formation of ZrCl2 and C2Cl6, above the b.p. formation of ZrCl4 and C;;
参考文献
Nippon Kagaku Zasshi, , vol. 81, p. 677 - 677
C. A., , p. 18410
