3,3'-二氨基二丙基胺 合成路线 （共 53 条）
反应条件
2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; sodium t-butanolate; bis(dibenzylideneacetone)-palladium(0) in 1,4-dioxane Heating; Title compound not separated from byproducts.;
参考文献
Averin, Alexei D.; Shukhaev, Anton V.; Golub, Svetlana L.; Buryak, Alexei K.; Beletskaya, Irina P.
反应条件
1: 83 percent / acetic acid / 1 h / Heating 2: 58 percent / K2CO3 / acetonitrile / 12 h / Heating 3: 85 percent / N2H4*H2O / ethanol / 2 h / Heating View Scheme
参考文献
Culf, Adrian S.; Melanson, Jennifer A.; Ouellette, Rodney J.; Briand, Glen G.
反应条件
1: 70 percent / sodium hydroxide / H2O / 1.) 1 hr., 5 deg C, 2.) r.t., 3 hrs. 2: 79 percent / tetrabutylammonium iodide, sodium hydroxide (50 percent) / toluene; H2O / 9 h / Heating View Scheme
参考文献
Luk'yanenko, N.G.; Basok, S.S.; Filonova, L.K.
反应条件
in 2-butoxy-ethanol T=60 - 170°C; 2 h; Inert atmosphere;
参考文献
WO2011/112594 A1, ;
反应条件
1: methanol / 20 °C / Inert atmosphere 2: triethylamine / ethanol / 20 °C 3: trifluoroacetic acid / dichloromethane / 2 h / 20 °C View Scheme
参考文献
Culf, Adrian S.; Melanson, Jennifer A.; Ouellette, Rodney J.; Briand, Glen G.
参考文献
Rothgery, E. F.; Niedenzu, K.
反应条件
in chloroform T=3°C; 0.0833333 h;
参考文献
Bell, Thomas W.; Anugu, Sreenivasa; Bailey, Patrick; Catalano, Vincent J.; Dey, Kaka; Drew, Michael G. B.; Duffy, Noah H.; Jin, Qi; Samala, Meinrado F.; Sodoma, Andrej; Welch, William H.; Schols, Dominique; Vermeire, Kurt
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反应条件
124481-62-5 3,7,11,18,22,26-六氮杂三环[26.2.2.213,16]三十四烷-13,15,28,30,31,33-己烯
反应条件
1: 95 percent / tetrahydrofuran / 5 h / 0 °C 2: 80 percent / LiAlH4 / tetrahydrofuran / 12 h / 50 °C View Scheme
参考文献
Pietraszkiewicz, Marek; Gasiorowski, Rafal
反应条件
hydrogenchloride in ethanol
参考文献
PRESIDENT AND FELLOWS OF HARVARD COLLEGE; CLARDY, Jon; BÖTTCHER, Thomas; LOSICK, Richard; KOLODKIN-GAL, Illana
参考文献
Hansen, John B.; Langvad, Eyvind; Frandsen, Flemming; Buchardt, Ole
