NH4NO3-NH3 in toluene soln. of TiCl4 added to alcohol with cooling and stirring, soln. added to NH4NO3-NH3 with stirring and cooling at 0-15°C; organic layer separated, solvent removed, product distilled under vacuum;
参考文献
Journal of applied chemistry of the USSR, , vol. 58, # 8 pt 2 p. 1678 - 1680