1-(4-苄氧基-苯基)-2-丙酮合成路线 (共 7 条)
反应条件
pyridine 6 h; Heating;
参考文献
THE GOVERNMENT OF THE UNITED STATES OF AMERICA AS REPRESENTED BY THE SECRETARY OF THE DEPARTMENT OF HEALTH AND HUMAN SERVICES
Patent: WO2008/22038 A1, 2008 ;
Location in patent: Page/Page column 39 ;
WO 2008/022038 A1
反应条件
tributylphosphine; water; diphenyldisulfane 1.) THF, room temp.; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 25, # 34 p. 3707 - 3710
反应条件
1: 77 percent / ethylenediamine / 4 h / Heating 2: 100 percent / sodium borohydride / propan-2-ol; tetrahydrofuran / 24 h / Ambient temperature 3: diphenyl disulphide, tributylphosphine / tetrahydrofuran / 3 h / Ambient temperature 4: water / tetrahydrofuran / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2243 - 2252
反应条件
1: 100 percent / sodium borohydride / propan-2-ol; tetrahydrofuran / 24 h / Ambient temperature 2: diphenyl disulphide, tributylphosphine / tetrahydrofuran / 3 h / Ambient temperature 3: water / tetrahydrofuran / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2243 - 2252
参考文献
Australian Journal of Chemistry, , vol. 20, p. 1413 - 1428
反应条件
Yield given. Multistep reaction;
参考文献
Archiv der Pharmazie, , vol. 325, # 12 p. 751 - 760
反应条件
hydrogen; palladium on activated charcoal in methanol T=23°C;
参考文献
Beecham Group P.L.C.
Patent: US4622342 A1, 1986 ;