2-(乙酰基硫代)苯甲酸合成路线 （共 12 条）
反应条件
T=230 - 300°C; P=15 - 17 Torr;
参考文献
Anschuetz; Rhodius
Chemische Berichte, 1914 , vol. 47, p. 2733
反应条件
T=300°C; P=15 - 17 Torr;
参考文献
Anschuetz; Rhodius
Chemische Berichte, 1914 , vol. 47, p. 2733
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Mayer,F.
Chemische Berichte, 1909 , vol. 42, p. 1133
反应条件
1.1: thionyl chloride; urea / toluene / 3 h / 10 - 110 °C 2.1: magnesium / ethanol; tetrachloromethane; diethyl ether / 3.5 h / |Reflux 2.2: 0.5 h / 20 °C 3.1: hydrogenchloride / ethanol / 3 h / |Reflux 4.1: hydrogenchloride / ethanol; water / 2 h / |Reflux View Scheme
参考文献
Arjunan; Santhanam; Sakiladevi; Marchewka; Mohan
Journal of Molecular Structure, 2013 , vol. 1037, p. 305 - 316
参考文献
Hinsberg
Chemische Berichte, 1910 , vol. 43, p. 652
反应条件
T=300°C; P=15 - 17 Torr;
参考文献
Anschuetz; Rhodius
Chemische Berichte, 1914 , vol. 47, p. 2733
Full Text Show Details
Mayer,F.
Chemische Berichte, 1909 , vol. 42, p. 1133
反应条件
pyridine
T=20°C; Acetylation; 10 h;
参考文献
Jung, Jae-Chul; Kim, Ju-Cheun; Park, Oee-Sook
Synthetic Communications, 2000 , vol. 30, # 7 p. 1193 - 1203
参考文献
Hinsberg
Chemische Berichte, 1910 , vol. 43, p. 652
反应条件
potassium hydroxide
T=20°C; 0.5 h;
参考文献
Kumar, Pradeep; Bodas, Mandar S
Tetrahedron, 2001 , vol. 57, # 48 p. 9755 - 9758
反应条件
1: 85 percent / hydriodic acid, hypophosphorous acid, conc. hydrochloric acid / 3 h / Heating
2: acetic acid
View Scheme
参考文献
Bhatt, M. Vivekananda; El Ashry, Shaker H.; Somayaji, Vishwanatha
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 6 p. 473 - 486
反应条件
in toluene
10 h; Heating;
参考文献
Kumar, Pradeep; Rao, Ashok T.; Pandey, Bipin
Journal of the Chemical Society, Chemical Communications, 1992 , # 21 p. 1580 - 1581
