2,3,4,5-四氟苯胺合成路线 （共 19 条）
反应条件
hydrogenchloride in water 2 h; Reflux;
参考文献
Safina, Larisa Yu.; Selivanova, Galina A.; Koltunov, Konstantin Yu.; Shteingarts, Vitalij D.
Tetrahedron Letters, 2009 , vol. 50, # 37 p. 5245 - 5247
反应条件
1: With [NiCl2(py)4]; zinc in 1-methyl-pyrrolidin-2-one; water T=70°C; 4 h; Inert atmosphere; 2: With sodium hydroxide in water T=20°C; 1 h;
参考文献
Prikhodko; Adonin; Parmon
Russian Chemical Bulletin, 2009 , vol. 58, # 11 p. 2304 - 2310
Izv. Akad. Nauk, Ser. Khim., 2009 , # 11 p. 2234 - 2239,6
反应条件
potassium carbonate in N,N-dimethyl-formamide Heating at 145°C, 6 h.;
参考文献
Gmelin Handbook: F: PerFHalOrg.7, 1, page 1 - 84
反应条件
1: NO2/HNO3, BF3 / tetrahydrothiophene 1,1-dioxide 2: H2 / Pd-C View Scheme
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 2323 - 2324
反应条件
hydrogenchloride; tin
参考文献
Tetrahedron, , vol. 23, p. 4719 - 4727
反应条件
1: dimethylformamide / Heating 2: H2SO4 3: aq. H2SO4 / Heating View Scheme
参考文献
Tetrahedron, , vol. 23, p. 4719 - 4727
反应条件
1: aq. H2SO4 / Heating 2: dimethylformamide / Heating 3: H2SO4 4: aq. H2SO4 / Heating View Scheme
参考文献
Tetrahedron, , vol. 23, p. 4719 - 4727
反应条件
sulfuric acid Heating;
参考文献
Tetrahedron, , vol. 23, p. 4719 - 4727
反应条件
1.1: |Reflux 2.1: zinc; [NiCl2(py)4] / 1-methyl-pyrrolidin-2-one; water / 4 h / 70 °C / |Inert atmosphere 2.2: 1 h / 20 °C View Scheme
参考文献
Russian Chemical Bulletin, , vol. 58, # 11 p. 2304 - 2310
Izv. Akad. Nauk, Ser. Khim., , # 11 p. 2234 - 2239,6
反应条件
1: H2SO4 2: aq. H2SO4 / Heating View Scheme
参考文献
Tetrahedron, , vol. 23, p. 4719 - 4727
