N-[4-(2-溴乙酰基)苯基]甲烷磺酰胺合成路线 （共 11 条）
反应条件
bromine; acetic acid T=55°C; 0.25 h; regiospecific reaction;
参考文献
Zanka, Atsuhiko; Kubota, Ariyoshi; Hirabayashi, Satoshi; Nakamura, Hitoshi
Organic Process Research and Development, 1998 , vol. 2, # 2 p. 71 - 77
反应条件
1: triethylamine / CH2Cl2 / 3 h / 25 °C 2: 81 percent / bromine; AlCl3 / CHCl3 / 0.5 h / 0 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 15, # 2 p. 1056 - 1061
反应条件
bromine; acetic acid in water T=55°C; 1 h; Large scale; regiospecific reaction;
参考文献
Organic Process Research and Development, , vol. 2, # 2 p. 71 - 77
反应条件
aluminium trichloride in carbon disulfide
参考文献
Journal of medicinal chemistry, , vol. 9, # 1 p. 88 - 97
反应条件
bromine; acetic acid T=55°C; 1 h; regiospecific reaction;
参考文献
Organic Process Research and Development, , vol. 2, # 2 p. 71 - 77
反应条件
pyridine; potassium carbonate; copper(l) chloride T=115°C; Ullmann Condensation; 6 h; Inert atmosphere; Reagent/catalystTime;
参考文献
Organic Process Research and Development, , vol. 2, # 2 p. 71 - 77
反应条件
1: dichloromethane / 1 h / 20 - 25 °C / |Large scale 2: bromine; acetic acid / water / 1 h / 55 °C / |Large scale View Scheme
参考文献
Organic Process Research and Development, , vol. 2, # 2 p. 71 - 77
反应条件
1: dichloromethane / 1 h / 20 - 25 °C / |Large scale 2: bromine; acetic acid / 6 h / 15 °C View Scheme
参考文献
Organic Process Research and Development, , vol. 2, # 2 p. 71 - 77
反应条件
bromine; acetic acid T=15°C; 6 h; regiospecific reaction;
参考文献
Organic Process Research and Development, , vol. 2, # 2 p. 71 - 77
反应条件
bromine; acetic acid T=15°C; 6 h; regiospecific reaction;
参考文献
Organic Process Research and Development, , vol. 2, # 2 p. 71 - 77
