反应条件
(C2H5)2CHOH; N,N,N',N'-tetramethylguanidine in deuterated toluene
byproducts: (C2H5)2CO; addn. of N,N,N'N'-tetramethylguanidine (1.1 equiv) to mixt. of (Bi(mesityl)(4-ClC6H4)3)(BF4) (1.1 equiv.), Et2CHOH (1 equiv.) and toluene-d8; stirring at room temp.; TLC analysis; concn. under reduced pressure, sepn. by chromy. (hexane-hexane/EtOAc or CH2Cl2);
参考文献
Matano, Yoshihiro; Suzuki, Takeshi; Iwata, Takaharu; Shinokura, Tomonori; Imahori, Hiroshi
Bulletin of the Chemical Society of Japan, 2008 , vol. 81, # 12 p. 1621 - 1628
