2-(3-N-邻苯二甲酰亚胺丙基)乙酰乙酸乙酯合成路线 (共 6 条)
反应条件
1: ethyl acetoacetate With potassium carbonate in acetone 1 h; Reflux; 2: 2-(3-iodopropyl)-1H-isoindolone-1,3(2H)-dione in acetone 255 h; Reflux;
参考文献
Prabhakar; Kumar, N. Vasanth; Reddy, M. Ravikanth; Sarma; Reddy, G. Om
Organic Process Research and Development, 1999 , vol. 3, # 3 p. 155 - 160
反应条件
potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in toluene 5 h; Heating;
参考文献
Kuang, Yunyan; Huang, Jian; Chen, Fener
Synthetic Communications, 2006 , vol. 36, # 11 p. 1515 - 1519
反应条件
1: potassium carbonate; TEBA / acetonitrile / 0.1 h / Heating; microwave irradiation 2: potassium carbonate / acetonitrile / 0.1 h / Heating; microwave irradiation View Scheme
参考文献
Synthetic Communications, , vol. 33, # 5 p. 741 - 747
反应条件
1.1: sodium iodide / acetone / 12 h / |Reflux 2.1: potassium carbonate / acetone / 1 h / |Reflux 2.2: 255 h / |Reflux View Scheme
参考文献
Organic Process Research and Development, , vol. 3, # 3 p. 155 - 160
反应条件
potassium carbonate in acetonitrile 0.1 h; Heatingmicrowave irradiation;
参考文献
Synthetic Communications, , vol. 33, # 5 p. 741 - 747
参考文献
Journal of the Chemical Society, , p. 7
Chemische Berichte, , vol. 42, p. 1241