4-苄氧基-3-甲氧基苯乙烯合成路线 （共 11 条）
反应条件
1: Methyltriphenylphosphonium bromide With potassium tert-butylate in tetrahydrofuran T=0 - 20°C; Inert atmosphere; 2: 4-benzyloxy-3-methoxy-benzaldehyde in tetrahydrofuran 2 h;
参考文献
Koolaji, Nooshin; Abu-Mellal, Abdallah; Tran, Van H.; Duke, Rujee K.; Duke, Colin C.
European Journal of Medicinal Chemistry, 2013 , vol. 63, p. 415 - 422
反应条件
sodium hydride in tetrahydrofuran T=80°C; Wittig reaction; 0.166667 h; microwave conditions;
参考文献
Su, Chung-Ren; Shen, Yuh-Chiang; Kuo, Ping-Chung; Leu, Yann-Lii; Damu, Amooru G.; Wang, Yea-Hwey; Wu, Tian-Shung
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 24 p. 6155 - 6160
反应条件
1.1: potassium carbonate / acetone / 3 h / Inert atmosphere; Reflux 2.1: n-butyllithium / tetrahydrofuran; hexanes / 1 h / 0 °C / Inert atmosphere 2.2: 3 h / 0 °C / Inert atmosphere View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 22, # 18-19 p. 1729 - 1735
反应条件
N-hexadecyl-N,N,N-trimethylammonium bromide; sodium hydroxide in dichloromethane T=80°C;
参考文献
Chemical Biology and Drug Design, , vol. 78, # 1 p. 101 - 111
反应条件
1.1: potassium carbonate / acetone / 3 h / Inert atmosphere; Reflux 2.1: n-butyllithium / tetrahydrofuran; hexanes / 1 h / 0 °C / Inert atmosphere 2.2: 3 h / 0 °C / Inert atmosphere View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 22, # 18-19 p. 1729 - 1735
反应条件
potassium hydroxide in ethanol Heating;
参考文献
Tetrahedron, , vol. 31, p. 235 - 238
反应条件
1: 87 percent / KI; K2CO3 / acetone 2: 77.2 percent / NaH / tetrahydrofuran / 0.17 h / 80 °C / microwave conditions View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 16, # 24 p. 6155 - 6160
反应条件
1: NaHCO3 / methanol 2: aq. KOH / ethanol / Heating View Scheme
参考文献
Tetrahedron, , vol. 31, p. 235 - 238
反应条件
hydrogen in methanol T=20°C; 7 h;
参考文献
Monguchi, Yasunari; Fujita, Yuki; Endo, Koichi; Takao, Shinobu; Yoshimura, Masatoshi; Takagi, Yukio; Maegawa, Tomohiro; Sajiki, Hironao
Chemistry - A European Journal, 2009 , vol. 15, # 4 p. 834 - 837
反应条件
1: With sodium tetrahydroborate; iodine in tetrahydrofuran
2: With sodium hydroxide; dihydrogen peroxide
参考文献
Su, Na; Wang, Zhen-Jun; Wang, Li-Zhong; Zhang, Xiao; Dong, Wei-Li; Wang, Hong-Xue; Li, Zheng-Ming; Zhao, Wei-Guang
Chemical Biology and Drug Design, 2011 , vol. 78, # 1 p. 101 - 111
