1: 1-iodo-2-nitro-benzene With phenyl-magnesium chloride in tetrahydrofuran T=-78°C; 2: boric acid trimethyl ester in tetrahydrofuran T=-78 - 20°C; 3: With hydrogenchloride in tetrahydrofuran
参考文献
ROHM AND HAAS ELECTRONIC MATERIALS KOREA LTD.; AHN, Hee Choon; CHO, Young Jun; KWON, Hyuck Joo; KIM, Bong Ok; KIM, Sung Min
Patent: WO2011/132865 A1, 2011 ;
Location in patent: Page/Page column 14 ;
1: With phenyl-magnesium chloride in tetrahydrofuran T=-60°C; 0.0833333 h; 2: With boric acid trimethyl ester in tetrahydrofuran T=-60°C; 0.5 h; 3: With hydrogenchloride in tetrahydrofuran T=-20°C;
参考文献
Collibee, Scott E.; Yu, Jiaxin
Tetrahedron Letters, 2005 , vol. 46, # 26 p. 4453 - 4455
