hydrogenchloride; mercury dichloride
bei der Destillation;
参考文献
Bunsen
Justus Liebigs Annalen der Chemie, 1841 , vol. 37, p. 23
Justus Liebigs Annalen der Chemie, 1842 , vol. 42, p. 18
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Baeyer
Justus Liebigs Annalen der Chemie, 1858 , vol. 107, p. 263
in deuterated toluene
Me2NAs(CH3)2 and C7H8-d8 were placed in a NMR tube; the tube was evacuated at -196°C and BCl3 condensed into it; NMR study of the reaction from -100°C to 25°C; mechanism discussed;; not isolated, detected by (11)B-, (13)C-, and (1)H-NMR spectroscopy;;
参考文献
Krannich, Larry K.; Kanjolia, Ravindra K.; Watkins, Charles L.
Journal of the Indian Chemical Society, 1985 , vol. 62, # 11 p. 795 - 799
in deuterated toluene
Me2NBCl2 and C7H8-d8 were placed in a NMR tube; the tube was evacuated at -196°C and Me2AsNMe2 condensed into it; the tube was sealed and agitated gently at -90°C; NMR study of the reaction from -90°C to 25°C;; not isolated, detected by (11)B-, (13)C-, and (1)H-NMR spectroscopy;;
参考文献
Krannich, Larry K.; Kanjolia, Ravindra K.; Watkins, Charles L.
Journal of the Indian Chemical Society, 1985 , vol. 62, # 11 p. 795 - 799
