2-巯基-5-甲氧基苯并噻唑合成路线 (共 10 条)
反应条件
1: With carbon disulfide 5 h; Reflux; 2: With hydrogenchloride in water
参考文献
YANG, Guangfu; ZHAO, Peiliang; HUANG, Wei; LIU, Zuming; WU, Hualong
Patent: US2010/292285 A1, 2010 ;
Location in patent: Page/Page column 2; 3 ;
反应条件
1: 5 h; Reflux; 2: With hydrogenchloride in water
参考文献
Huazhong Normal University; Zhejiang Bosta Cropscience Co., Ltd.
Patent: EP2301925 A1, 2011 ;
Location in patent: Page/Page column 3; 4 ;
反应条件
carbon disulfide; sodium hydroxide in ethanol
反应条件
in N,N-dimethyl-formamide T=120°C; 0.25 h; microwave irradiation;
参考文献
Huang, Wei; Tan, Ying; Ding, Ming-Wu; Yang, Guang-Fu
Synthetic Communications, 2007 , vol. 37, # 3 p. 369 - 376
反应条件
sulfuryl dichloride in tetrahydrofuran
参考文献
WO2007/146066 A2, ;
Page/Page column 89 ;
反应条件
sodium hydroxide; ethanol
参考文献
Li, Xiaokai; Srinivasan, Sharan R.; Connarn, Jamie; Ahmad, Atta; Young, Zapporah T.; Kabza, Adam M.; Zuiderweg, Erik. R. P.; Sun, Duxin; Gestwicki, Jason E.
ACS Medicinal Chemistry Letters, 2013 , vol. 4, # 11 p. 1042 - 1047
参考文献
Berry, Craig R.; Zificsak, Craig A.; Gibbs, Alan C.; Hlasta, Dennis J.
Organic Letters, 2007 , vol. 9, # 21 p. 4099 - 4102
反应条件
bromine in chloroform T=0°C; 1.5 h;
参考文献
Ramurthy, Savithri; Aikawa, Mina; Amiri, Payman; Costales, Abran; Hashash, Ahmad; Jansen, Johanna M.; Lin, Song; Ma, Sylvia; Renhowe, Paul A.; Shafer, Cynthia M.; Subramanian, Sharadha; Sung, Leonard; Verhagen, Joelle
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 11 p. 3286 - 3289
反应条件
in sodium hydroxide; water; acetone
参考文献
Merck and Co., Inc.
Patent: US4454148 A1, 1984 ;
反应条件
laccase from Trametes versicolor; oxygen; ABTS diammonium salt in methanol
T=20°C; pH=4.4; 24 h; Green chemistryEnzymatic reaction;
参考文献
Abdel-Mohsen, Heba T.; Sudheendran, Kavitha; Conrad, Juergen; Beifuss, Uwe
Green Chemistry, 2013 , vol. 15, # 6 p. 1490 - 1495