in further solvent(s)
byproducts: glyme, Cd(CH3)2; Cd compd. added to GeI4 in 1,2-dibromoethane, standing for 1 h, periodically vented to vac.; after volatile germanes recovered, concd., sepd.;
参考文献
Krause, L. J.; Morrison, J. A.
Journal of the American Chemical Society, 1981 , vol. 103, # 11 p. 2995 - 3001
addition of CF3 radicals to gaseous GeBr4 and condensation at -130°C;; purification by gas chromatography;;
参考文献
Lagow et al.
Journal of the American Chemical Society, 1975 , vol. 97, p. 518
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Gmelin Handbook: F: PerFHalOrg.4, 4.2.1, page 165 - 169