1: With N,N,N',N,-tetramethylethylenediamine; sec.-butyllithium in diethyl ether; cyclohexane
T=-78°C; Metallation; 0.5 h;
2: With acetic acid in diethyl ether
Hydrolysis; Further stages.;
参考文献
Hammerschmidt, Friedrich; Hanbauer, Martin
Journal of Organic Chemistry, 2000 , vol. 65, # 19 p. 6121 - 6131
Zimin,M.G. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1978 , vol. 27, p. 436 - 437
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1978 , vol. 27, p. 499 - 500