1-环丙基-1-苯基乙醇合成路线 （共 19 条）
反应条件
1: bromobenzene With iodine; magnesium in tetrahydrofuran T=20°C; 2 h; Inert atmosphere; 2: cyclopropane carboxylic acid cyanide in tetrahydrofuran T=0 - 20°C; Grignard reaction; 1 h; Inert atmosphere; 3: With water in tetrahydrofuran Grignard reaction; Inert atmosphere;
参考文献
Organic Letters, , vol. 13, # 24 p. 6504 - 6507
反应条件
bis(acetylacetonate)nickel(II) in tetrahydrofuran T=0°C;
参考文献
Chemistry Letters, , # 11 p. 1149 - 1150
反应条件
samarium; mercury dichloride in tetrahydrofuran T=-78 - 20°C;
参考文献
Journal of Organic Chemistry, , vol. 54, # 15 p. 3525 - 3532
反应条件
bis(acetylacetonate)nickel(II); methyllithium in tetrahydrofuran T=0°C;
参考文献
Chemistry Letters, , # 11 p. 1149 - 1150
反应条件
in toluene T=80°C; 1 h;
参考文献
Synthesis, , # 9 p. 1127 - 1130
反应条件
in tetrahydrofuran; diethyl ether T=20°C; 3 h;
参考文献
Chemistry - A European Journal, , vol. 20, # 9 p. 2440 - 2444
参考文献
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, , vol. 43, p. 1164
Chem. Zentralbl., , vol. 83, # I p. 1458
反应条件
1: 24 percent / (diacetoxy)iodobenzene; I2 / CH2Cl2 / 0.25 h / 20 °C / Irradiation 2: tetrahydrofuran View Scheme
参考文献
Journal of Organic Chemistry, , vol. 70, # 17 p. 6820 - 6826
参考文献
Zhurnal Obshchei Khimii, , vol. 20, p. 581,587; engl. Ausg. S. 613, 618
反应条件
1: 78 percent / KHSO4 / toluene / Heating 2: 1) O2, cumene hydroperoxide, 2) LiAlH4 / 1) cumene, heating View Scheme
参考文献
Journal fuer Praktische Chemie - Practical Applications and Applied Chemistry (Germany), , vol. 341, # 1 p. 52 - 58
