2-叔丁氧羰基氨基丙烯酸甲酯合成路线 (共 79 条)
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=28°C; 24 h;
参考文献
Ramapanicker, Ramesh; Mishra, Roli; Chandrasekaran, Srinivasan
Journal of Peptide Science, 2010 , vol. 16, # 3 p. 123 - 125
反应条件
in diethyl ether T=-10°C; 5 h;
参考文献
Tetrahedron Letters, , vol. 25, # 26 p. 2759 - 2762
反应条件
potassium carbonate in acetonitrile T=20°C; Addition; Michael addition;
参考文献
Journal of the Chemical Society, Perkin Transactions 1, , # 19 p. 3317 - 3324
反应条件
potassium carbonate in acetonitrile T=20°C; Addition; Michael addition; Substitution;
参考文献
Journal of the Chemical Society, Perkin Transactions 1, , # 19 p. 3317 - 3324
反应条件
potassium carbonate in acetonitrile T=20°C; Addition; Michael addition; Substitution;
参考文献
Journal of the Chemical Society, Perkin Transactions 1, , # 19 p. 3317 - 3324
反应条件
1: 94 percent / pyridine, Et3N / CH2Cl2 / 1.) 10 min, 2.) 2.5 h 2: 76 percent / CuCl, EDCI / CHCl3 / 5 h View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 16 p. 2485 - 2499
反应条件
tetraethylammonium chloride; triethyl amine hydrochloride in acetonitrile detosylation; Electrolysis;
参考文献
Ferreira, Paula M.T.; Maia, Hernani L.S.; Monteiro, Luis S.; Sacramento, Joana
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 24 p. 3697 - 3703
反应条件
in diethyl ether T=-60°C; 5 h;
参考文献
Tetrahedron Letters, , vol. 25, # 26 p. 2759 - 2762
反应条件
1: ethyl acetate With n-butyllithium; diisopropylamine in tetrahydrofuran; hexane T=-78°C; Metallation; 1 h; 2: Boc-Ser(TBDMS)OMe in tetrahydrofuran; hexane T=-78°C; Elimination; Claisen condensation; 12 h;
参考文献
Boesche, Uwe; Nubbemeyer, Udo
Tetrahedron, 1999 , vol. 55, # 22 p. 6883 - 6904
反应条件
potassium carbonate in acetonitrile T=20°C; Addition; Michael addition; Substitution;
参考文献
Journal of the Chemical Society, Perkin Transactions 1, , # 19 p. 3317 - 3324