2-叔丁氧羰基氨基丙烯酸甲酯合成路线 （共 79 条）
反应条件
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; copper(l) chloride in 4-(dicyanomethylene)-2-methyl-6-(4-dimethylaminostyryl)-4H-pyran T=20°C; 72 h;
参考文献
Breslin, Henry J.; Cai, Chaozhong; He, Wei; Kavash, Robert W.
Patent: US2005/203143 A1, 2005 ;
Location in patent: Page/Page column 45 ;
US 20050203143 A1
反应条件
O-(2,4,6-trimethylbenzenesulfonyl)hydroxylamine; potassium carbonate in water; N,N-dimethyl-formamide T=20°C; 0.05 h;
参考文献
Bernardes, Goncalo J. L.; Chalker, Justin M.; Errey, James C.; Davis, Benjamin G.
Journal of the American Chemical Society, 2008 , vol. 130, # 15 p. 5052 - 5053
反应条件
triethylamine in dichloromethane T=20°C; 3 h;
参考文献
PROZYMEX A/S; PEDERSEN, John; LAURITZEN, Conni
Patent: WO2012/130299 A1, 2012 ;
Location in patent: Page/Page column 108 ;
WO 2012/130299 A1
反应条件
N'-(3-dimethylaminopropyl)-N-ethylcarbodiimide; copper(l) chloride in chloroform 5 h; Ambient temperature;
参考文献
Andruszkiewicz, Ryszard; Grzybowska, Jolanta; Wojciechowska, Hanna
Polish Journal of Chemistry, 1981 , vol. 55, # 1 p. 67 - 71
反应条件
lithium diethylcuprate in diethyl ether T=-60°C; 3 h;
参考文献
Bajgrowicz, J. A.; Hallaoui, A. El; Jacquier, R.; Pigiere, Ch.; Viallefont, Ph.
Tetrahedron, 1985 , vol. 41, # 10 p. 1833 - 1845
反应条件
O-(2,4,6-trimethylbenzenesulfonyl)hydroxylamine; potassium carbonate in water; N,N-dimethyl-formamide T=20°C; 0.166667 h;
参考文献
Bernardes, Goncalo J. L.; Chalker, Justin M.; Errey, James C.; Davis, Benjamin G.
Journal of the American Chemical Society, 2008 , vol. 130, # 15 p. 5052 - 5053
反应条件
oxygen; O-(2,4,6-trimethylbenzenesulfonyl)hydroxylamine; potassium carbonate in water; N,N-dimethyl-formamide T=20°C; 0.0333333 h;
参考文献
Journal of the American Chemical Society, , vol. 130, # 15 p. 5052 - 5053
反应条件
4 A molecular sieve; toluene-4-sulfonic acid in 1,1,2-trichloroethylene 8 h; Heating;
参考文献
Gladiali; Pinna
Tetrahedron Asymmetry, 1991 , vol. 2, # 7 p. 623 - 632
反应条件
methanesulfonyl chloride; triethylamine in dichloromethane T=0 - 20°C; 2 h;
参考文献
Collier, Philip N.; Campbell, Andrew D.; Patel, Ian; Raynham, Tony M.; Taylor, Richard J. K.
Journal of Organic Chemistry, 2002 , vol. 67, # 6 p. 1802 - 1815
反应条件
tris-(dimethylamino)-phosphine in tetrahydrofuran T=20°C; 0.0833333 h;
参考文献
Wang, Hua; Zhang, Jiming; Xian, Ming
Journal of the American Chemical Society, 2009 , vol. 131, # 37 p. 13238 - 13239
