GRANULAR BLUE 粒蓝相似物合成路线 （共 24 条）
反应条件
1: 79 percent / toluene / 1.5 h / Heating
2: 76 percent / 10 percent sodium methanolate / methanol / 2 h / Ambient temperature
3: 78 percent / triethylphosphite / 20 h / Heating
4: 1) ethanol; 2) NH3 / 1) CHCl3; 2) ethanol
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
反应条件
1: 82 percent
2: 49 percent / 10 percent sodium methanolate / methanol / 0.5 h / Ambient temperature
3: 78 percent / triethylphosphite / 20 h / Heating
4: 1) ethanol; 2) NH3 / 1) CHCl3; 2) ethanol
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
反应条件
1: 85 percent / pyridine, thionylchloride / diethyl ether / 3 h / Ambient temperature
2: 82 percent
3: 49 percent / 10 percent sodium methanolate / methanol / 0.5 h / Ambient temperature
4: 78 percent / triethylphosphite / 20 h / Heating
5: 1) ethanol; 2) NH3 / 1) CHCl3; 2) ethanol
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
反应条件
1: 8 percent / HF / 20 h / 45 - 50 °C
2: quinoline
3: 1) ethanol; 2) NH3 / 1) CHCl3; 2) ethanol
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
反应条件
1: 66 percent / quinoline
2: 1) ethanol; 2) NH3 / 1) CHCl3; 2) ethanol
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
反应条件
1: 63 percent / 18 percent HCl / 0.17 h / Heating
2: 49 percent / 10 percent sodium methanolate / methanol / 0.5 h / Ambient temperature
3: 78 percent / triethylphosphite / 20 h / Heating
4: 1) ethanol; 2) NH3 / 1) CHCl3; 2) ethanol
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
反应条件
1: 86 percent / Zn / acetic acid / 0.25 h / Heating
2: 66 percent / quinoline
3: 1) ethanol; 2) NH3 / 1) CHCl3; 2) ethanol
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
反应条件
1: quinoline
2: 1) ethanol; 2) NH3 / 1) CHCl3; 2) ethanol
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
反应条件
1: 97 percent / 2 N NaOH / ethanol / 1 h / 5 - 10 °C
2: 63 percent / 18 percent HCl / 0.17 h / Heating
3: 49 percent / 10 percent sodium methanolate / methanol / 0.5 h / Ambient temperature
4: 78 percent / triethylphosphite / 20 h / Heating
5: 1) ethanol; 2) NH3 / 1) CHCl3; 2) ethanol
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
反应条件
1: 49 percent / 10 percent sodium methanolate / methanol / 0.5 h / Ambient temperature
2: 78 percent / triethylphosphite / 20 h / Heating
3: 1) ethanol; 2) NH3 / 1) CHCl3; 2) ethanol
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
