GRANULAR BLUE 粒蓝相似物合成路线 （共 24 条）
反应条件
1: K2CO3 / dimethylformamide / 3 h / 155 - 160 °C
2: 92 percent / piperidine / 24 h / 100 °C
3: 78 percent / triethylphosphite / 20 h / Heating
4: 1) ethanol; 2) NH3 / 1) CHCl3; 2) ethanol
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
反应条件
1: 72 percent / K2CO3 / dimethylformamide / 3 h / 155 - 160 °C
2: 92 percent / piperidine / 24 h / 100 °C
3: 78 percent / triethylphosphite / 20 h / Heating
4: 1) ethanol; 2) NH3 / 1) CHCl3; 2) ethanol
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
反应条件
1: K2CO3 / dimethylformamide / 3 h / 155 - 160 °C
2: 92 percent / piperidine / 24 h / 100 °C
3: 78 percent / triethylphosphite / 20 h / Heating
4: 1) ethanol; 2) NH3 / 1) CHCl3; 2) ethanol
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
反应条件
1: 92 percent / piperidine / 24 h / 100 °C
2: 78 percent / triethylphosphite / 20 h / Heating
3: 1) ethanol; 2) NH3 / 1) CHCl3; 2) ethanol
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
反应条件
1: 96 percent / KOH / 0.25 h / Heating
2: 97 percent / 2 N NaOH / ethanol / 1 h / 5 - 10 °C
3: 63 percent / 18 percent HCl / 0.17 h / Heating
4: 49 percent / 10 percent sodium methanolate / methanol / 0.5 h / Ambient temperature
5: 78 percent / triethylphosphite / 20 h / Heating
6: 1) ethanol; 2) NH3 / 1) CHCl3; 2) ethanol
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
反应条件
1: 52 percent / HF / 30 h / 45 - 50 °C
2: 86 percent / Zn / acetic acid / 0.25 h / Heating
3: 66 percent / quinoline
4: 1) ethanol; 2) NH3 / 1) CHCl3; 2) ethanol
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
反应条件
1: 46 percent / conc. HCl / 0.07 h / Heating
2: 68 percent / conc. H2SO4, HNO3 / 2 h / 5 - 10 °C
3: 8 percent / HF / 20 h / 45 - 50 °C
4: quinoline
5: 1) ethanol; 2) NH3 / 1) CHCl3; 2) ethanol
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
反应条件
1: 68 percent / conc. H2SO4, HNO3 / 2 h / 5 - 10 °C
2: 8 percent / HF / 20 h / 45 - 50 °C
3: quinoline
4: 1) ethanol; 2) NH3 / 1) CHCl3; 2) ethanol
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
反应条件
1: 52 percent / HF / 30 h / 45 - 50 °C
2: 86 percent / Zn / acetic acid / 0.25 h / Heating
3: 66 percent / quinoline
4: 1) ethanol; 2) NH3 / 1) CHCl3; 2) ethanol
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
反应条件
1: 49 percent / 10 percent sodium methanolate / methanol / 0.5 h / Ambient temperature
2: 78 percent / triethylphosphite / 20 h / Heating
3: 1) ethanol; 2) NH3 / 1) CHCl3; 2) ethanol
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
